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Last update: Kubová Petra Ing. (30.01.2018)
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Last update: Kubová Petra Ing. (30.01.2018)
Students will be able to understand: 1. Principles, technical configurations and application potential of sample preparation methods 2. Principles, technical configurations and application potential of gas and liquid chromatography including the application of conventional detectors 3. Principles, technical configurations and application potential of mass spectrometric methods based on various principles of ion separation |
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Last update: Poustka Jan prof. Dr. Ing. (13.09.2023)
Pawliszyn J.: Solid phase microextraction: Theory and Practice. Wiley-VCH, Inc. NY, USA, ISBN 0-471-19034-9, 1997. Dean, J.R.: Extraction Methods for Environmental Analysis, J.Wiley&Sons, Ltd., Chichester, Anglie, ISBN 0-471-98287-3, 1998. Grob, R.L. (Editor): Modern Practice of Gas Chromatography, J.Wiley&Sons, Inc., NY, USA, ISBN 0-471-59700-7, 1995. Willoughby, R., Sheehan, E., Mitrovich, S.: A Global View of LC/MS: How to Solve Your Most Challenging Analytical Problems, Global View Publishing, Pittsburg, Pennsylvania, USA, ISBN 0-9660813-0-7, 1998. Snyder,L.R., Kirkland, J.J., Glajch, J.L.: Practical HPLC Method Development, J.Wiley&Sons, Inc., NY, USA, ISBN 0-471-00703-X, 1997. Scientific papers. |
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Last update: Poustka Jan prof. Dr. Ing. (13.09.2023)
https://e-learning.vscht.cz/ |
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Last update: Vlčková Martina Ing. (02.02.2018)
Within the extent of the syllabus. |
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Last update: Kubová Petra Ing. (30.01.2018)
1. General characteristics of analytical procedure and classification of techniques 2. Purge & trap, head space, supercritical fluid extraction 3. Liquid-liquid extraction, liquid micro-extraction 4. Solid-liquid extraction, various means of implementation (ASE-PLE, MASE) 5. Solid phase extraction 6. Solid phase micro-extraction 7. Adsorption chromatography, dispersive solid phase extraction (MSPD, QuEChERS) 8. Gel permeation chromatography 9. Gas chromatography - factors influencing separation, injection techniques 10. Gas chromatography - columns, detectors 11. Gas chromatography - large volume injection; GCxGC 12. Liquid chromatography - factors influencing separation 13. Liquid chromatography - columns, detectors 14. Mass spectrometry |
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Last update: Kubová Petra Ing. (30.01.2018)
No requirements |
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Last update: Kubová Petra Ing. (30.01.2018)
Successful completion of a written examination. |
Teaching methods | ||||
Activity | Credits | Hours | ||
Konzultace s vyučujícími | 0.5 | 14 | ||
Účast na přednáškách | 1.5 | 42 | ||
Příprava na přednášky, semináře, laboratoře, exkurzi nebo praxi | 0.5 | 14 | ||
Příprava na zkoušku a její absolvování | 1.5 | 42 | ||
4 / 4 | 112 / 112 |