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Last update: Pátková Vlasta (15.11.2018)
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Last update: Pátková Vlasta (15.11.2018)
At the end, the students will understand the principles of the analytical methods applied for trace element analysis, know the practical rules of laboratory work in trace analysis and achieve key competences to carry out these analyses using various analytical methods. Students will be able to predict possible interferences encountered in a variety of methods in specific cases and to propose an appropriate solution of the problem. They will be able to choose the suitable way of sample preparation, the measurement technique and its main conditions with regard to the sample’s nature. |
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Last update: Pátková Vlasta (15.11.2018)
R Aras N.K., Ataman O. Y.: Trace Element Analysis of Food and Diet, RSC Publishing , Cambridge, UK, 2006, ISBN 0-85404-576-7 A Comprehensive Analytical Chemistry Vol. 30, 1996 (editor R. Lobinski), ISBN 978044482368-7; Vol 33, 2000 (editor J.A. Caruso) ISBN 9780444500472; Vol 41 (editor Z. Mester) ISBN 9780444511010, Elsevier |
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Last update: Pátková Vlasta (15.11.2018)
http://www.rsc.org/journals-books-databases/about-journals/jaas/ |
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Last update: Pátková Vlasta (15.11.2018)
Lectures. |
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Last update: Pátková Vlasta (15.11.2018)
There are no requirements for students concerning the tests of their knowlwdge during the semester. |
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Last update: Pátková Vlasta (15.11.2018)
The content of subject is divided into three parts. The first part focuses on the background and conditions of trace elements analysis and includes (a) general problems of trace analysis, (b) sampling strategy, (c) sample preparation (decomposition and optional ways) and (d) pre-concentration method and separation of trace elements. The second part is focused on the instrumental methods of trace elements determination and includes the following topics (e) atomic absorption spectrometry, (f) methods of generating of volatile compounds of trace elements, (g) optical emission spectrometry including ICP-OES and its applications, (h) inductively coupled plasma mass spectrometry (ICP-MS) and (i) electrochemical methods. The third part is devoted to the chemical species of trace elements in biological materials and the methods of speciation analysis and includes (j) separation techniques in speciation analysis and (k) the use of ICP-MS in speciation analysis. |
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Last update: Pátková Vlasta (15.11.2018)
There are no initial requirements. |
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Last update: Pátková Vlasta (15.11.2018)
There are no prerequisites. |
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Last update: Pátková Vlasta (15.11.2018)
Oral exam. |