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Last update: Mestek Oto prof. Ing. CSc. (12.08.2018)
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Last update: Mestek Oto prof. Ing. CSc. (06.08.2018)
Students completing the course will acquire theoretical knowledge of the methods of elemental analysis using optical spectrometry (absorption, emission and fluorescence), X-ray spectrometry and mass spectrometry. They will be familiar with the various methods of sample preparation and problems of cleanness in trace laboratory. |
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Last update: Mestek Oto prof. Ing. CSc. (10.10.2018)
R: Cullen M.: Atomic Spectroscopy in Elemental Analysis, Blackwell 2004, ISBN 1-84127-333-3
R: Broekaert José A.C.: Analytical Atomic Spectrometry with Flames and Plasmas, Wiley 2002, ISBN 978-3-527-31282-5
R: Becker J.S.: Inorganic Mass Spectrometry, Principles and Applications, Wiley 2007, ISBN 978-0-470-01200-0 |
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Last update: Mestek Oto prof. Ing. CSc. (12.08.2018)
Elaboration of individual project - literatury research or laboratory work. An oral examination. |
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Last update: Mestek Oto prof. Ing. CSc. (06.08.2018)
1. Structure of atoms.
2. Interaction of electrons and electromagnetic radiation, width and intensity of spectral lines.
3. Fundamentals of optics, construction of monochromators and polychromators, construction of radiation detectors.
4. Atomic absorption spectrometry, basic instrumentation - radiation sources, atomizers.
5. Atomic absorption spectrometry: interference and background correction, signal optimization and processing.
6. Atomic absorption spectrometry: special techniques - hydride generation, mercury determination, electrodeposition.
7. Atomic fluorescence spectrometry.
8. Flame emission spectrometry, spectrometry with electric arc and spark excitation, rotating electrode spectroscopy, spectroscopy with glow discharge.
9. Inductively coupled and DC plasma optical emission spectrometry, LIBS
10. Inductively coupled plasma mass spectrometry: basic instrumentation - ion optics, ion filters and detectors.
11. Inductively coupled plasma mass spectrometry: interference and methods of their elimination; special techniques - laser ablation, analysis of nanoparticles, connection with electrothermal evaporation.
12. Hyphenated techniques in speciation analysis of trace elements.
13. X-ray fluorescence spectrometry.
14. Preparation of samples for elemental trace analysis, principles of work in a trace laboratory. |
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Last update: Mestek Oto prof. Ing. CSc. (19.08.2018)
Basic knowledge of analytical chemistry, physics and mathematics. |
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Last update: Mestek Oto prof. Ing. CSc. (12.08.2018)
Acknowledgement of literary research or passing labs and acknowledgement of protocols. To complete the oral exam, the student must successfully answer two questions from the list of questions. |