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Last update: Poustka Jan prof. Dr. Ing. (19.01.2018)
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Last update: Fialová Jana (19.12.2017)
Students will be able to understand: 1. Principles, technical configurations and application potential of sample preparation methods 2. Principles, technical configurations and application potential of gas and liquid chromatography including the application of conventional detectors 3. Principles, technical configurations and application potential of mass spectrometric methods based on various principles of ion separation |
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Last update: Poustka Jan prof. Dr. Ing. (13.09.2023)
Pawliszyn J.: Solid phase microextraction: Theory and Practice. Wiley-VCH, Inc. NY, USA, ISBN 0-471-19034-9, 1997 Dean, J.R.: Extraction Methods for Environmental Analysis, J.Wiley&Sons, Ltd., Chichester, Anglie, ISBN 0-471-98287-3, 1998 Grob, R.L. (Editor): Modern Practice of Gas Chromatography, J.Wiley&Sons, Inc., NY, USA, ISBN 0-471-59700-7, 1995 Willoughby, R., Sheehan, E., Mitrovich, S.: A Global View of LC/MS: How to Solve Your Most Challenging Analytical Problems, Global View Publishing, Pittsburg, Pennsylvania, USA, ISBN 0-9660813-0-7, 1998 Snyder,L.R., Kirkland, J.J., Glajch, J.L.: Practical HPLC Method Development, J.Wiley&Sons, Inc., NY, USA, ISBN 0-471-00703-X, 1997 Scientific papers |
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Last update: Poustka Jan prof. Dr. Ing. (13.09.2023)
https://e-learning.vscht.cz/ |
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Last update: Vlčková Martina Ing. (30.01.2018)
Within the extent of the syllabus. |
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Last update: Fialová Jana (19.12.2017)
1. General characteristics of analytical procedure and classification of techniques 2. Purge & trap, head space, supercritical fluid extraction 3. Liquid-liquid extraction, liquid micro-extraction 4. Solid-liquid extraction, various means of implementation (ASE-PLE, MASE) 5. Solid phase extraction 6. Solid phase micro-extraction 7. Adsorption chromatography, dispersive solid phase extraction (MSPD, QuEChERS) 8. Gel permeation chromatography 9. Gas chromatography - factors influencing separation, injection techniques 10. Gas chromatography - columns, detectors 11. Gas chromatography - large volume injection; GCxGC 12. Liquid chromatography - factors influencing separation 13. Liquid chromatography - columns, detectors 14. Mass spectrometry |
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Last update: Fialová Jana (19.12.2017)
No requirements |
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Last update: Poustka Jan prof. Dr. Ing. (19.01.2018)
Successful completion of a written examination. |
Teaching methods | ||||
Activity | Credits | Hours | ||
Konzultace s vyučujícími | 0.5 | 14 | ||
Účast na přednáškách | 1.5 | 42 | ||
Příprava na přednášky, semináře, laboratoře, exkurzi nebo praxi | 0.5 | 14 | ||
Příprava na zkoušku a její absolvování | 1.5 | 42 | ||
4 / 4 | 112 / 112 |