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Spectroscopic Characterization of Heterogeneous Catalysts - D105018

Title:	Spektroskopická charakterizace heterogenních katalyzátorů
Guaranteed by:	Department of Inorganic Technology (105)
Faculty:	Faculty of Chemical Technology
Actual:	from 2011 to 2013
Semester:	both
Points:	0
E-Credits:	0
Examination process:
Hours per week, examination:	0/0, other [HT]
Capacity:	winter:unknown / unknown (unknown) summer:unknown / unknown (unknown)
Min. number of students:	unlimited
State of the course:	taught
Language:	Czech
Teaching methods:	full-time
Teaching methods:	full-time
Level:
Note:	course is intended for doctoral students only you can enroll for the course in winter and in summer semester

Guarantor:	Sobalík Zdeněk doc. Ing. CSc.

Examination dates Schedule

Annotation -

The aim of the course is to make students acquainted with modern approaches to the characterization of heterogeneous catalysts by spectroscopic methods, with emphasis on experiments under conditions in situ or Operands. In addition to repeating of method principle and the process of the catalysts preparation, the main procedures of structural and surface analysis of catalysts in the process of their preparation, using and deactivation are discussed. Lectures are supplemented with examples of solutions of structural problems and dealing with the relationship between the structure and activity of heterogeneous catalysts.

Last update: ROZ105 (22.04.2014)

Aim of the course -

Students will be able to

analyze the structure and surface properties of heterogeneous catalysts

independently evaluate and discuss the obtained data

choose the appropriate combination of methods for the characterization of any catalyst

Last update: ROZ105 (22.04.2014)

Course completion requirements -

Processing and defense of seminary work.

Last update: ROZ105 (22.04.2014)

Literature -

R: B.A. Averill, J.A. Moulijn, R.A. van Santen, P.W.N.M. van Leeuwen: Catalysis: An Integrated Approach (Studies in Surface Science and Catalysis, Vol. 123) (Elsevier)

R: J. W. Niemantsverdriet: Spectroscopy in Catalysis (Wiley)

A: M. Che and J.C. Védrine: Characterization of Solid Materials and Heterogeneous Catalysts: From Structure to Surface Reactivity (Wiley)

Last update: ROZ105 (22.04.2014)

Syllabus -

1. Preparation of catalyst and its characterization, overview of available methods

2. Electron spectroscopy (XPS, UPS, AES, EELS)

3. Ion spectroscopy (SIMS, SNMS, LEIS)

4. Vibration spectroscopy (infrared, Raman)

5. Temperature-programmed techniques(TPR, TPO, TPD)

6. Difraction techniques (XRD, EXAFS) and microscopy (TEM, SEM, STEM, STM, AFM)

7. Exkursion to "ÚFCH JH" with demonstration of most of the described techniques

Last update: ROZ105 (22.04.2014)