SubjectsSubjects(version: 963)
Course, academic year 2013/2014
  
Structural Analysis - N110006
Title: Strukturní analýza
Guaranteed by: Department of Organic Chemistry (110)
Faculty: Faculty of Chemical Technology
Actual: from 2013 to 2014
Semester: summer
Points: summer s.:4
E-Credits: summer s.:4
Examination process: summer s.:
Hours per week, examination: summer s.:2/1, C+Ex [HT]
Capacity: 95 / 32 (unknown)
Min. number of students: unlimited
State of the course: taught
Language: Czech
Teaching methods: full-time
Teaching methods: full-time
Level:  
Additional information: http://www.vscht.cz/eso/pracoviste-110_cze.html
Note: course can be enrolled in outside the study plan
enabled for web enrollment
Guarantor: Böhm Stanislav doc. Ing. CSc.
Examination dates   Schedule   
Annotation -
The basic aim of this course is to gain knowledge about principles and practical use of spectroscopic method in the field of organic chemistry.
Last update: BOHM (03.11.2005)
Aim of the course -

Students will be able to :

understand basic principles of spectroscopic methods in organic chemistry

use NMR, IR , UV-VIS and MS spectra in structure analysis of organic compounds

Last update: Cibulka Radek (28.11.2013)
Literature -

R: Böhm S., Smrčková S.: Strukturní analýza organických sloučenin, VŠCHT, 1995. 8070802359

A: Williams D.H., Fleming I.: Spectroscopic methods in organic chemistry. 5. vydání. DH Williams & I Fleming. 9780077091477

Last update: BOHM (26.08.2013)
Syllabus -

1. Overview of molecular spectroscopy methods, base conception and principles

2. NMR, base info, main conceptions, range of application

3. 1H NMR in organic structure analysis

4. 13C NMR in organic structure analysis

5. Special techniques of NMR

6. 2D NMR - COSY, HETCOR

7. Infrared spectroscopy, base conception and principles

8. Characteristic vibrations and „finger print“ region

9. Applications in structure analysis

10. UV-VIS spectroscopy, base conception and principles

11. Practical applications in structure analysis

12. Mass spectra, fundamental of method, experimental arrangement

13. Ionisation technique, separation techniques, basic types of fragmentation

14. Application in structure analysis of organic compounds

Last update: BOHM (27.04.2005)
Learning resources -

Teaching support to lectures at the lecturer

Last update: Cibulka Radek (26.08.2013)
Registration requirements -

Organic Chemistry II, Physics

Last update: BOHM (26.08.2013)
Teaching methods
Activity Credits Hours
Účast na přednáškách 1 28
Příprava na přednášky, semináře, laboratoře, exkurzi nebo praxi 1 28
Příprava na zkoušku a její absolvování 1.5 42
Účast na seminářích 0.5 14
4 / 4 112 / 112
Coursework assessment
Form Significance
Oral examination 100

 
VŠCHT Praha