Subjects

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Analysis of Natural Bioactive Compounds: Laboratory - N323046

Title:	Laboratoř analýzy biologicky aktivních přírodních látek
Guaranteed by:	Department of Food Analysis and Nutrition (323)
Faculty:	Faculty of Food and Biochemical Technology
Actual:	from 2013 to 2014
Semester:	summer
Points:	summer s.:3
E-Credits:	summer s.:3
Examination process:	summer s.:
Hours per week, examination:	summer s.:0/4, MC [HT]
Capacity:	unknown / 7 (unknown)
Min. number of students:	unlimited
State of the course:	taught
Language:	Czech
Teaching methods:	full-time
Teaching methods:	full-time
Level:
Note:	course can be enrolled in outside the study plan enabled for web enrollment

Guarantor:	Pulkrabová Jana prof. Ing. Ph.D. Stránská Milena prof. Ing. Ph.D.
Class:	Specializační laboratoř

Examination dates Schedule

Annotation -

The course Analysis of Natural Bioactive Compounds: Laboratory is designed for students who have completed the course Analysis of Natural Bioactive Compounds. The aim of the course is to introduce to students selected modern techniques for sample preparation, development and optimization of analyte separation, detection of compounds, data handling and interpretation. Laboratories are designed as single handed activities of students on their projects, the first part is based on a literature review and proposal of a suitable analytical procedure and after the consultation with the teacher, the project can be realized in the laboratory. The measured data are evaluated and interpreted in the final report.

Last update: Pulkrabová Jana (03.07.2013)

Aim of the course -

Students will be able to:

prepare and plan the experimental work in the modern laboratory.

under the leadership to realise the sample preparation and final instrumental analysis of organic compounds.

process and interpret the measured data.

Last update: TAJ323 (23.08.2013)

Literature -

R: Otles S. (ed.): Handbook of Food Analysis Instruments. CRC Press, Boca Raton, USA, 2009, e-zdroj VŠCHT, ISBN 9781420045666.

R: W.M.A. Niessen: Current Practice of Gas Chromatography-Mass Spectrometry. Marcel Dekker, Inc., USA, 2001, ISBN 9780824704735.

R: W.M.A. Niessen: Liquid Chromatography-Mass Spectrometry. CRC Press, Boca Raton, USA, 2006, ISBN 978-0-8247-4082-5.

R: Watson J. T., Sparkman O. D.: Introduction to Mass Spectrometry. Wiley, Chichester, Velká Británie, 2007, ISBN 978-0-470-51634-8.

Last update: Pulkrabová Jana (03.07.2013)

Syllabus -

1. Introduction, organization of laboratories, laboratory safety, project assignment

2.- 3. Preparation of project (selection methods, literature search

4.- 11. Laboratory work - work on the project

12.- 14. Data processing, preparation of the final project report

Last update: TAJ323 (28.08.2013)

Learning resources -

http://web.vscht.cz/cajkat/ABAPL.html

http://www.chem.arizona.edu/massspec/

http://www.ionsource.com/tutorial/spectut/spec1.htm

http://www.chemguide.co.uk/analysis/masspecmenu.html

http://webbook.nist.gov/chemistry/

http://www.chemspider.com/

http://www.massbank.jp/

http://metlin.scripps.edu/

Last update: Pulkrabová Jana (03.07.2013)

Registration requirements -

Analysis of Natural Bioactive Compounds

Last update: Pulkrabová Jana (03.07.2013)

Teaching methods
	Activity	Credits	Hours
	Účast v laboratořích (na exkurzi nebo praxi)	2	56
	Příprava na přednášky, semináře, laboratoře, exkurzi nebo praxi	0.5	14
	Práce na individuálním projektu	0.5	14
		3 / 3	84 / 84

Coursework assessment
Form	Significance
Regular attendance	50
Defense of an individual project	50