Subjects

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Analysis of Complex Hydrocarbon Mixtures - D215004

Title:	Analýza komplexních uhlovodíkových směsí
Guaranteed by:	Department of Petroleum Technology and Alternative Fuels (215)
Faculty:	Faculty of Environmental Technology
Actual:	from 2011 to 2022
Semester:	both
Points:	0
E-Credits:	0
Examination process:
Hours per week, examination:	0/0, other [HT]
Capacity:	winter:unknown / unknown (unknown) summer:unknown / unknown (unknown)
Min. number of students:	unlimited
State of the course:	taught
Language:	Czech
Teaching methods:	full-time
Level:
Note:	course is intended for doctoral students only can be fulfilled in the future you can enroll for the course in winter and in summer semester

Guarantor:	Pospíšil Milan prof. Ing. CSc.

Examination dates Schedule

Annotation -

The course introduces students to modern methods of analysis of multicomponent hydrocarbon mixtures using the effective chromatographic separation methods as well as spectrometric methods (UV / VIS, FTIR, MS, NMR). Students will be introduced with examples of analysis of real hydrocarbon fractions and products as well as samples of the contaminated environment.

Last update: Pospíšil Milan (08.11.2015)

Syllabus -

1. Introduction, comparison between standardized and non-standardized instrumental analytical methods to analyse multicomponent hydrocarbon mixtures

2. Problems of qualitative and quantitative analysis of multicomponent hydrocarbon mixtures, the hydrocarbon matrix complexity influence on accuracy of the determination

3. Options for pre-separation and pre-concentration of samples to final analysis - an appropriate combination of separation procedures

4. Gas chromatography - instrumentation, columns, detectors

5. Gas Chromatography - examples of analysis, problem solving

6. High performance liquid chromatography - instrumentation, columns, detectors

7. High performance liquid chromatography - examples of analysis, troubleshooting

8. Other methods of liquid chromatography - gel permetion chromatography, complexation chromatography

9. Mass Spectrometry - instrumentation

10. Mass spectrometry - principles of interpretation of the spectra

11. UV / VIS spectrometry - instrumentation, examples of analysis

12. FTIR - instrumentation, basic interpretation of spectra, examples of analysis

13. NMR - instrumentation, basic interpretation of spectra, examples of analysis

14. Analysis of sulfur, nitrogen and oxygen heterocompounds in hydrocarbon samples

Last update: Pospíšil Milan (08.11.2015)

Learning outcomes -

Students will gain an overview of the instrumental analytical equipment and suitable combinations of the methods for pretreatment and simplification of samples before final analysis, not least as the modalities for interpretation of experimental data.

Last update: Pospíšil Milan (08.11.2015)

Registration requirements -

Analytical chemistry, Fuel analysis

Last update: Pospíšil Milan (08.11.2015)