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Instrumental methods used in analysis of organic and inorganic compounds in water including sample preparation are discussed: separation methods (chromatography - GC, GC-MS, HPLC, capillary isotachophoresis, ionic chromatography), spectral methods (AAS, ICP), total organic carbon (TOC), adsorbable and extractable organically bound halogens (AOX, EOX) and hydrocarbon index. Applicability of the methods is demonstrated during excursions.
Last update: Janda Václav (28.08.2013)
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Students will be able to: use instrumental analytical methods for water analysis. Last update: Janda Václav (28.08.2013)
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R: M. Popl, J. Fähnrich: Analytická chemie životního prostředí (Environmental analytical chemistry), VŠCHT Praha 1999, ISBN 80-7080-336-3 A: J. Pawlyszin: Solid phase microextraction; theory and practice, Wiley-VCH, New York 1997, ISBN 0-471-19034-9 Last update: Janda Václav (02.10.2013)
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Zkouška se koná jen písemnou formou na konci semestru. Opravnou zkoušku je možné konat během zkouškového období. Last update: Janda Václav (15.11.2012)
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1. Introduction, guidelines, standards and required detection limits 2. Organic compounds, chromatographic methods (GC and HPLC), detection systems 3. Preconcentration and enrichment techniques for organic compounds 4. Derivatization, analyses of pesticides, PAHs, PCBs, volatile chlorinated hydrocarbons, haloforms, hydrocarbons 5. Capillary isotachophoresis 6. Heavy metals, atomic absorption spectroscopy 7. Total organic carbon, dissolved organic carbon, biochemical oxygen demand 8. Adsorbable and extractable organic chlorine (halogens) 9. Ionic chromatography 10. Gene probes 11. Excursion, demonstration 12. Excursion, demonstration 13. Excursion, demonstration 14. Test Last update: TAJ217 (28.11.2005)
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http://www.vscht.cz/homepage/tvp/index Last update: Janda Václav (21.08.2013)
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Analytical chemistry I Last update: TAJ217 (28.08.2013)
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Teaching methods | ||||
Activity | Credits | Hours | ||
Účast na přednáškách | 1 | 28 | ||
Příprava na zkoušku a její absolvování | 2 | 56 | ||
3 / 3 | 84 / 84 |
Coursework assessment | |
Form | Significance |
Regular attendance | 30 |
Examination test | 70 |