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Development of skills obtained in the preceding course, column chromatography and spectroscopical characterization of products.
Last update: Hladíková Jana (03.01.2018)
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Students will be able to: combine the theoretical knowledge with experimental results understand the system of organic synthesis - reaction planning, building a reaction apparatus, carrying out a reaction, isolation and characterization of products write laboratory protocols Last update: Hladíková Jana (03.01.2018)
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Odevzdání preparátů, úspěšné absolvování testu. Last update: Kundrát Ondřej (16.02.2018)
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R: Šilhánková a kol.: Laboratoř organické chemie, Vydavatelství VŠCHT, 2000, dotisk 2007, 8070803959 Last update: Himl Michal (14.08.2024)
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1. Laboratory safety and first aid instructions. 2. One-step syntheses of various organic substances, isolation and identification of products. 3. Multi-step syntheses. 4. Operations under anhydrous conditions. 5. Operations on semimicroscale. 6. Organic solvents, extraction, drying, evaporation. 7. Crystallization and filtration. 8. Column chromatography. 9. Thin layer chromatography. 10. Distillation under ambient pressure. 11. Distillation under reduced pressure. 12. Melting point determination. 13. Gas chromatography. 14. NMR spectrometry. Last update: Hladíková Jana (03.01.2018)
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Laboratory instructions https://e-learning.vscht.cz/course/view.php?id=2182 Last update: Himl Michal (14.08.2024)
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Organic chemistry: Laboratory I Last update: Hladíková Jana (03.01.2018)
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Organic chemistry: Laboratory I Last update: Hladíková Jana (03.01.2018)
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Teaching methods | ||||
Activity | Credits | Hours | ||
Účast v laboratořích (na exkurzi nebo praxi) | 2 | 56 | ||
Příprava na přednášky, semináře, laboratoře, exkurzi nebo praxi | 1 | 28 | ||
Práce na individuálním projektu | 1 | 28 | ||
4 / 4 | 112 / 112 |