Subjects

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NMR spectroscopy in Natural Compounds - N342010

Title:	NMR pro studium přírodních látek
Guaranteed by:	Department of Chemistry of Natural Compounds (342)
Faculty:	Faculty of Food and Biochemical Technology
Actual:	from 2021
Semester:	summer
Points:	summer s.:3
E-Credits:	summer s.:3
Examination process:	summer s.:
Hours per week, examination:	summer s.:2/1, MC [HT]
Capacity:	unknown / unknown (unknown)
Min. number of students:	unlimited
State of the course:	cancelled
Language:	Czech
Teaching methods:	full-time
Teaching methods:	full-time
Level:
Is provided by:	M342008
Additional information:	http://doc. Ing. R. Hrabal, CSc.

Guarantor:	Hrabal Richard prof. Ing. CSc. Dvořáková Hana Ing. CSc. Prchal Jan Ing. Ph.D.
Is interchangeable with:	M342008

Examination dates Schedule

Annotation -

The purpose of the course is to teach students the fundaments of Nuclear magnetic resonance spectroscopy. It is designed for NMR users to be able to choose a proper NMR experiment, to set it up on an NMR spectrometer, process the results and interpret the spectra. The course is divided into three sections, the first one is about physical background of NMR, the second one is devoted to principles of interpretation of NMR spectra and the last one should help students to orient themselves in numerous applications of NMR spectroscopy. Students must work out their own projects to successfully pass the course.

Last update: TAJ342 (18.12.2013)

Aim of the course -

Students will be able to:

Understand the basics of NMR spectroscopy and its possibilities for solving common problems in chemists’ practice

Successfully set simple 1D and 2D experiments on NMR spectrometer

Process NMR data

Optimally interpret resulting spectra

Last update: TAJ342 (30.09.2013)

Literature -

R: H. Friebolin: Basic One- and Two-Dimensional NMR Spectroscopy, Wiley-VCH, 4. edition, 2005

A: H. Günther: NMR Spectrsocopy John Wileay and Sons, 2.edition, 2001

Last update: TAJ342 (30.09.2013)

Syllabus -

1. Basic concepts, principle of pulse experiments

2. Two- and multidimensional NMR

3. Nuclear relaxation, chemical exchange, NOE effect

4. Construction and basis of operation of NMR spectrometers

5. Interpretation of NMR spectra, calculations, databases

6. Conformational analysis I

7. Conformational analysis II

8. Chemical exchange

9. Multi-nuclear NMR and its application for solving particular problems

10. Examination project assignment

11. NMR of biologically active systems

12. Study of non-bonding interactions

13. Quantitative NMR, magnetic resonance imaging

14. Solid-state NMR

Last update: TAJ342 (30.09.2013)

Learning resources -

https://clab.vscht.cz/nmr/vyuka/nmr_pl

Last update: Prchal Jan (21.09.2018)

Registration requirements -

Basic knowledge of mathematics, physics, and chemistry

Last update: TAJ342 (30.09.2013)

Teaching methods
	Activity	Credits	Hours
	Obhajoba individuálního projektu	0.5	14
	Příprava na přednášky, semináře, laboratoře, exkurzi nebo praxi	0.5	14
	Práce na individuálním projektu	0.5	14
	Příprava na zkoušku a její absolvování	1	28
	Účast na seminářích	0.5	14
		3 / 3	84 / 84

Coursework assessment
Form	Significance
Report from individual projects	20
Oral examination	80