SubjectsSubjects(version: 995)
Course, academic year 2023/2024
  
   
Specialized Laboratory - Inorganic Chemistry - M101005
Title: Laboratoř specializace - anorganická chemie
Form of teaching: laboratory practicals
Guaranteed by: Department of Inorganic Chemistry (101)
Faculty: Faculty of Chemical Technology
Actual: from 2019 to 2024
Duration in semesters: 1
Semester: winter
Points: winter s.:7
E-Credits: winter s.:7
Examination process: winter s.:
Hours per week, examination: winter s.:0/10, MC [HT]
Capacity: unknown / unlimited (unknown)
Maximum number of enrolled students: unlimited
Min. number of students: unlimited
State of the course: taught
Language: Czech
Teaching methods: full-time
Level:  
Repeated enrollment: - / - / - / 9
Note: course can be enrolled in outside the study plan
enabled for web enrollment
Guarantor: Nekvindová Pavla doc. Ing. Ph.D.
Class: Základní laboratoře
Classification: Chemistry > Inorganic Chemistry
Interchangeability : N101021
Examination dates   Schedule   
This subject contains the following additional online materials
Annotation -
The students will get acquainted with the research issue of Inorganic Chemistry Department. The preparation and characterization of various forms of inorganic materials. e.i. thin layers as bulk materials, powders, isomers of coordination compounds will be practiced. The materials characterization using modern techniques as DSC / TGA, AFM, X-ray, fluorescence spectrometry, mode spectroscopy. The aim of the practical exercises is a quick orientation in the scheduled lab, results obtaining and evaluation or search of general relationships between the determined data.
Last update: Pátková Vlasta (10.01.2018)
Literature -

There are work instructions at the members of inorganic chemistry department.(http://www.vscht.cz/ach/vyuka).

Last update: Pátková Vlasta (10.01.2018)
Requirements to the exam -

Each task is accompanied by laboratory protocol and evaluated by individual supervisor. Graded credit corresponds to the average of obtained marks and give it laboratories guarantee.

Last update: Pátková Vlasta (10.01.2018)
Syllabus -

Laboratory practice is carried out by students at the Department of Inorganic Chemistry. From the tasks offered, the student will do eight to twelve (selection takes into account the difficulty) laboratory tasks that must be completed during the semester.

The tasks will be selected from the following:

1. Processing and analysis of experimental data

2. Differectial scanning calorimetry of PbTiO3 – determination of heat capacity and thermodynamic characteristics of a feroelectric transition

3. Synthesis of transition metals perovskites by sol-gel methods

4. Measuring of luminiscence and absorption of optically active materials: preparation and characterisation of optically active materials

5. Simulation of lead azide concentration measurement in a waste water from the production of explosives

6. Synthesis and characterisation of geometric and linkage isomers of cobalt(III) complexes

7. Measuring of physical properties of thermoelectric cobalt-based mixed oxides

8. Graphene - synthesis by exfoliation of graphite oxide and its characterisation

9. Evaluation of unpaired electrons number in a paramagnetic complex

10. Electrochemical and spectroelectrochemicaal properties of ferrocene

11. Characterisation of isomers or alotropes by Raman spectroscopy and XRD

12. Scanning electron microscopy

13. Growth of high-temperature superconducting crystals of REBCO

14. Basic techniques of work with polarizing microscope

Last update: Jakeš Vít (03.09.2026)
Learning resources -

http://www.vscht.cz/ach/magisterske

http://www.vscht.cz/ach/výzkum

Last update: Pátková Vlasta (10.01.2018)
Learning outcomes -

Students will be able to:

quickly orientate themselves in the new special issue

characterize inorganic materials using modern techniques

observe and evaluate the obtained experimental data

search general context

Last update: Pátková Vlasta (10.01.2018)
Entry requirements -

General and Inorganic Chemistry I

Laboratory of Inorganic Chemistry I

Laboratory of Chemistry and Materials Technology

Last update: Pátková Vlasta (10.01.2018)
Registration requirements -

General and inorganic chemistry I

Inorganic chemistry : Laboratory I

Last update: Pátková Vlasta (10.01.2018)
 
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