SubjectsSubjects(version: 955)
Course, academic year 2019/2020
  
Organic Chemistry Laboratory I - AB110005
Title: Organic Chemistry Laboratory I
Guaranteed by: Department of Organic Chemistry (110)
Faculty: Faculty of Chemical Technology
Actual: from 2019 to 2019
Semester: both
Points: 3
E-Credits: 3
Examination process:
Hours per week, examination: 0/4, MC [HT]
Capacity: winter:unknown / unknown (unknown)
summer:unknown / unknown (unknown)
Min. number of students: unlimited
State of the course: not taught
Language: English
Teaching methods: full-time
Teaching methods: full-time
Level:  
Additional information: http://Do termínů laboratoří se musí studenti přihlásit prostřednictvím SIS jako na termín zkoušky z Laboratoří OCH I
Note: deregister from the exam date if a requisite was not fulfilled
course can be enrolled in outside the study plan
enabled for web enrollment
you can enroll for the course in winter and in summer semester
Guarantor: Kozmík Václav Ing. CSc.
Class: Základní laboratoře
Pre-requisite : {x}, {x}
Interchangeability : N110002, N110002A, N110502, Z110002
Examination dates   Schedule   
This subject contains the following additional online materials
Annotation -
Students will learn about laboratory safety, basic laboratory equipment and experimental procedures used in organic chemistry. Working on several simple organic syntheses, students will acquire the requisite skills for the preparation and characterization of organic compounds. Final grade is based not only on the performance in the laboratory, but also on the knowledge of simple calculations (stoichiometry and preparation of solutions) and the chemical principles of procedures carried out.
Last update: Kubová Petra (06.03.2019)
Aim of the course -

Students will be able to:

work safely in organic laboratory

carry out basic laboratory operations

combine the theoretical knowledge with experimental results

understand the system of organic synthesis - reaction planning, building a reaction apparatus, carrying out a reaction, isolation and characterization of products

write laboratory protocols

Last update: Kubová Petra (06.03.2019)
Literature -

R: J. W. Zubrick, The Organic Chem Lab Survival Manual: A Student's Guide to Techniques, 5th Ed., Wiley 2001.0471387320

Last update: Kubová Petra (06.03.2019)
Learning resources -

Laboratory instructions

Last update: Kubová Petra (06.03.2019)
Syllabus -

1. Laboratory safety and first aid instructions.

2. Laboratory rules, recordkeeping, protocols, essential calculations.

3. Basic laboratory equipment.

4. Building of reaction apparatuses.

5. Crystallization and filtration.

6. Organic solvents, extraction, drying, evaporation.

7. Stirring and heating under reflux.

8. One-step syntheses of various organic substances, isolation and identification of products.

9. Multi-step syntheses.

10. Operations under anhydrous conditions.

11. Distillation under ambient pressure.

12. Distillation under reduced pressure.

13. Melting point determination.

14. Gas chromatography.

Last update: Kubová Petra (06.03.2019)
Entry requirements -

Organic chemistry I or Organic Chemistry A and Inorganic Chemistry: Laboratory I.

Last update: Kubová Petra (06.03.2019)
Registration requirements -

Organic chemistry I or Organic Chemistry A and Inorganic Chemistry: Laboratory I.

Last update: Kubová Petra (06.03.2019)
Course completion requirements - Czech

Odevzdání preparátů, úspěšné absolvování testu.

Last update: Kubová Petra (06.03.2019)
 
VŠCHT Praha