|
|
|
||
Last update: Kubová Petra Ing. (22.01.2018)
|
|
||
Last update: Kubová Petra Ing. (22.01.2018)
Students will be able to: Describe and explain the principles and instrumentation of following techniques: photoelectron spectroscopy, Auger spectroscopy, X-ray fluorescence analysis, electron microscopy, scanning probe microscopy, X-ray, electron and neutron diffraction, secondary ion mass spectrometry, infrared and Raman microspectrometry and NMR spectrometry/relaxometry focusing on solids. Know examples of practical applications of individual techniques of structural and surface analysis. |
|
||
Last update: Matějka Pavel prof. Dr. RNDr. (21.02.2018)
R:Modern Instrumental Analysis, ed. S. Ahuja, N. Jespersen, Comprehensive Analytical Chemistry Vol. 47 (2006), p. 1-864, ISBN: 978-0-444-52259-7, https://www.sciencedirect.com/science/handbooks/0166526X/47 (available online at VSCHT)
A:Non-Destructive Microanalysis of Cultural Heritage materials, ed. S. Ahuja, N. Jespersen, Comprehensive Analytical Chemistry Vol. 42 (2004), p. 1-800, ISBN: 978-0-444-50738-9, https://www.sciencedirect.com/science/handbooks/0166526X/42 (available online at VSCHT)
A:R.L. McCreery: Raman Spectroscopy for Chemical Analysis, Wiley 2000, Online ISBN: 9780471721642, http://onlinelibrary.wiley.com/book/10.1002/0471721646 (available online at VSCHT)
A:L. A. Casper, C. J. Powell: Industrial Applications of Surface Analysis, vol. 199, ACS 1982, eISBN: 9780841209411, https://pubs.acs.org/doi/book/10.1021/bk-1982-0199 (available online at VSCHT)
A:Sam Zhang, Lin Li, Ashok Kumar: Materials Characterization Techniques, CRC Press Boca Raton 2009, ISBN 978-1-4200-4294-8 |
|
||
Last update: Kubová Petra Ing. (22.01.2018)
electronic materials - slides for lectures - http://www.vscht.cz/anl/matejka/#povrch |
|
||
Last update: Matějka Pavel prof. Dr. RNDr. (21.02.2018)
1. Fundamental terms of structural and surface analysis 2. Surface analysis methods based on electron detection (XPS, UPS) 3. Surface analysis methods based on electron detection (Auger spectroscopy) 4. Methods of electron microscopy and chemical analysis (EDX, WDX) 5. Methods of scanning probe microscopy (AFM, STM, SNOM) 6. Surface analysis methods based on ion detection (SIMS) 7. Methods of X-ray diffraction 8. Electron and neutron diffraction 9. Techniques of infrared and Raman spectrometry 10. Infrared and Raman microspectrometry, mapping and imaging 11. Surface-enhanced vibrational spectroscopies 12. NMR spectroscopy and molecular structure 13. Solid-state NMR spectroscopy 14. NMR analysis in inhomogeneous fields, mobile NMR |
|
||
Last update: Kubová Petra Ing. (22.01.2018)
none |
|
||
Last update: Matějka Pavel prof. Dr. RNDr. (21.02.2018)
It is compulsory to pass a written test and final oral examination. |
Teaching methods | ||||
Activity | Credits | Hours | ||
Konzultace s vyučujícími | 0.5 | 14 | ||
Účast na přednáškách | 1 | 28 | ||
Příprava na přednášky, semináře, laboratoře, exkurzi nebo praxi | 0.5 | 14 | ||
Příprava na zkoušku a její absolvování | 1 | 28 | ||
3 / 3 | 84 / 84 |