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Last update: Pátková Vlasta (19.11.2018)
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Last update: Pátková Vlasta (19.11.2018)
The students will be able to:
analyze powder pattern in Highscore Plus software, manipulate background, manual and automatic peak search, PDF4+ search perform semiquantitative phase analysis of mixture of phases using method of corundum numbers(RIR values) basics of Rietveld refinement, calculation of theoretical powder pattern. |
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Last update: Kubová Petra Ing. (30.11.2018)
R: Manual of Highscore Plus. R: Manual of Mercury. R: Manual of search-match program in Cambridge Structure Database.
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Last update: Pátková Vlasta (19.11.2018)
https://clab.vscht.cz/rtg-en http://reference.iucr.org/dictionary/ https://www.iucr.org/education/resources |
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Last update: Pátková Vlasta (19.11.2018)
lectures, exercises on manipulation and evaluation of real samples and their respective diffraction patterns |
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Last update: Pátková Vlasta (19.11.2018)
The following subjects will be explained in detail: 1. CIF based theoretical powder calculation in Highscore Plus. 2. Quantitative analysis using Rietveld's method. 3. Analysis of amorphous content in powder sample. 4. Size of crystallites, Hall-Williamson graph. 5. Advanced PDF4+ search. 6. Advanced CSD search. 7. Output of graphical results, Mercury and Ortep software. |
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Last update: Pátková Vlasta (19.11.2018)
none |
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Last update: Pátková Vlasta (19.11.2018)
Oral exam, prove skills working with real powder pattern. |