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Last update: Pátková Vlasta (15.11.2018)
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Last update: Pátková Vlasta (15.11.2018)
Students will be able to understand:
1. Principles, technical configurations and application potential of sample preparation methods
2. Principles, technical configurations and application potential of gas and liquid chromatography including the application of conventional detectors
3. Principles, technical configurations and application potential of mass spectrometric methods based on various principles of ion separation |
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Last update: Pátková Vlasta (15.11.2018)
R: Grob, R.L. (Editor) : Modern Practice of Gas Chromatography, J.Wiley&Sons, Inc., NY, USA, ISBN 0-471-59700-7, 1995
R: Dean, J.R. : Extraction Methods for Environmental Analysis, J.Wiley&Sons, Ltd., Chichester, Anglie, ISBN 0-471-98287-3, 1998
R: J. Pawliszyn: Solid phase microextraction: Theory and Practice. Wiley-VCH, Inc. . NY, USA, ISBN 0-471-19034-9, 1997
R: Willoughby, R., Sheehan, E., Mitrovich, S.: A Global View of LC/MS: How to Solve Your Most Challenging Analytical Problems, Global View Publishing, Pittsburg, Pennsylvania, USA, 1998.
R: Snyder,L.R., Kirkland, J.J., Glajch, J.L.: Practical HPLC Method Development, J.Wiley&Sons, Inc., NY, USA, ISBN 0-471-00703-X, 1997
A: Rood, D.: A Practical Guide to the Care Maintenance and Troubleshooting of Capillary Gas Chromatographic Systems, Hüthig GmbH, Heidelberg, Německo, ISBN 3-7785-2319-8, 1995
A: Scientific papers |
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Last update: Pátková Vlasta (15.11.2018)
Course outlines: http://web.vscht.cz/poustkaj |
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Last update: Pátková Vlasta (15.11.2018)
Lectures, consultations, self-study. |
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Last update: Pátková Vlasta (15.11.2018)
No requirements. |
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Last update: Pátková Vlasta (15.11.2018)
1. Overview of analytical methods and techniques in analytical procedures 2. Isolation methods in gas phase - purge & trap (PT), head space (HS) 3. Supercritical fluid extraction (SFE) 4. Liquid extraction – techniques: liquid-liquid extraction (LLE), liquid-solid extraction (LSE) 5. Liquid extraction at elevated temperature and pressure (ASE-PLE, MASE) 6. Solid phase extraction (SPE); solid phase micro-extraction (SPME) 7. Adsorption chromatography (LSC); gel permeation chromatography (GPC) 8. Dispersive solid phase extraction (MSPD, QuEChERS) 9. Gas chromatography – parameters; separation process, injection techniques; columns, detectors; GCxGC 10. Liquid chromatography – parameters; separation process, columns, detectors 11. Mass spectrometry – ionisation; mass analyzers, spectra interpretation |
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Last update: Pátková Vlasta (15.11.2018)
Basic knowledge of the fields: general chemistry, inorganic chemistry, organic chemistry, analytical chemistry. |
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Last update: Pátková Vlasta (15.11.2018)
No requirements. |
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Last update: Pátková Vlasta (15.11.2018)
Exam - written test. |