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Lectures are focused on selected analytical methods used in pharmaceutical industry. Solid state techniques, polymorphism, solvatomorphism, mixtures, etc. are accented.
Last update: Kubová Petra (03.01.2018)
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The students will be able to:
be oriented in basic crystallography and in selected analytical techniques; choose optimal method to analyse API's or related impurities, considering the nature od the compounds either crystalline obr amorphous, polymorph transformations, co-crystals, mixtures, etc.; analyse relative and absolute configuration. Last update: Kubová Petra (03.01.2018)
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R:Kraus I.,Struktura a vlastnosti krystalů,Academia,Praha,1993,802000372X Last update: Kubová Petra (03.01.2018)
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1. Macroscopic assembly And symmetry od solid state compounds 2. Microscopic organization And symmetry in solid state 3. Single crystal X-ray analysis 4. X-ray powder analysis 5. Quality parameters of X-ray data, software available 6. Databases CSD, PDB, PDF 7. X-ray fluorescence analysis 8. Solid state NMR 9. IR and Raman spectroscopy 10. Thermal methods - TG, DTA, DSC, HSM, DVS
Excursions: single crystal X-ray analysis powder and fluorescence X-ray analysis IR and Raman spectroscopy Thermal methods Last update: Kubová Petra (03.01.2018)
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Electronical version of study materials Last update: Kubová Petra (03.01.2018)
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Pro zápis tohoto předmětu je nutno mít minimálně zapsán předmět N108022 Last update: Kubová Petra (03.01.2018)
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No pre-requisites Last update: Kubová Petra (03.01.2018)
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Teaching methods | ||||
Activity | Credits | Hours | ||
Účast na přednáškách | 1 | 28 | ||
Příprava na přednášky, semináře, laboratoře, exkurzi nebo praxi | 1 | 28 | ||
Příprava na zkoušku a její absolvování | 1 | 28 | ||
3 / 3 | 84 / 84 |
Coursework assessment | |
Form | Significance |
Oral examination | 100 |