SubjectsSubjects(version: 855)
Course, academic year 2019/2020
  
Organic Chemistry: Laboratory I - B110005
Title: Laboratoř organické chemie I
Guaranteed by: Department of Organic Chemistry (110)
Actual: from 2019
Semester: both
Points: 3
E-Credits: 3
Examination process:
Hours per week, examination: 0/4 MC [hours/week]
Capacity: winter:unknown / unknown (unknown)
summer:unknown / unknown (unknown)
Min. number of students: unlimited
Language: Czech
Teaching methods: full-time
Level:  
For type: Bachelor's
Additional information: http://Do termínů laboratoří se musí studenti přihlásit prostřednictvím SIS jako na termín zkoušky z Laboratoří OCH I
Note: deregister from the exam date if a requisite was not fulfilled
course can be enrolled in outside the study plan
enabled for web enrollment
you can enroll for the course in winter and in summer semester
Guarantor: Kozmík Václav Ing. CSc.
Pre-requisite : {x}, {x}
Interchangeability : N110002, N110002A, N110502, Z110002
Annotation -
Last update: Kubová Petra Ing. (04.12.2017)
Students will learn about laboratory safety, basic laboratory equipment and experimental procedures used in organic chemistry. Working on several simple organic syntheses, students will acquire the requisite skills for the preparation and characterization of organic compounds. Final grade is based not only on the performance in the laboratory, but also on the knowledge of simple calculations (stoichiometry and preparation of solutions) and the chemical principles of procedures carried out.
Aim of the course -
Last update: Kubová Petra Ing. (04.12.2017)

Students will be able to:

work safely in organic laboratory

carry out basic laboratory operations

combine the theoretical knowledge with experimental results

understand the system of organic synthesis - reaction planning, building a reaction apparatus, carrying out a reaction, isolation and characterization of products

write laboratory protocols

Literature -
Last update: Kubová Petra Ing. (04.12.2017)

R: J. W. Zubrick, The Organic Chem Lab Survival Manual: A Student's Guide to Techniques, 5th Ed., Wiley 2001.0471387320

Learning resources -
Last update: Kubová Petra Ing. (04.12.2017)

Laboratory instructions

Syllabus -
Last update: Kubová Petra Ing. (04.12.2017)

1. Laboratory safety and first aid instructions.

2. Laboratory rules, recordkeeping, protocols, essential calculations.

3. Basic laboratory equipment.

4. Building of reaction apparatuses.

5. Crystallization and filtration.

6. Organic solvents, extraction, drying, evaporation.

7. Stirring and heating under reflux.

8. One-step syntheses of various organic substances, isolation and identification of products.

9. Multi-step syntheses.

10. Operations under anhydrous conditions.

11. Distillation under ambient pressure.

12. Distillation under reduced pressure.

13. Melting point determination.

14. Gas chromatography.

Entry requirements -
Last update: Kubová Petra Ing. (04.12.2017)

Organic chemistry I or Organic Chemistry A and Inorganic Chemistry: Laboratory I.

Registration requirements -
Last update: Kubová Petra Ing. (04.12.2017)

Organic chemistry I or Organic Chemistry A and Inorganic Chemistry: Laboratory I.

Course completion requirements - Czech
Last update: Kundrát Ondřej Ing. Ph.D. (16.02.2018)

Odevzdání preparátů, úspěšné absolvování testu.

Teaching methods
Activity Credits Hours
Účast v laboratořích (na exkurzi nebo praxi) 2 56
Příprava na přednášky, semináře, laboratoře, exkurzi nebo praxi 1 28
3 / 3 84 / 84
Coursework assessment
Form Significance
Regular attendance 40
Report from individual projects 30
Continuous assessment of study performance and course -credit tests 30

 
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