SubjectsSubjects(version: 895)
Course, academic year 2021/2022
  
Structural Analysis - B110007
Title: Strukturní analýza
Guaranteed by: Department of Organic Chemistry (110)
Actual: from 2021
Semester: summer
Points: summer s.:4
E-Credits: summer s.:4
Examination process: summer s.:
Hours per week, examination: summer s.:2/1 C+Ex [hours/week]
Capacity: unknown / unknown (unknown)
Min. number of students: unlimited
Language: Czech
Teaching methods: full-time
Level:  
For type:  
Note: course can be enrolled in outside the study plan
enabled for web enrollment
Guarantor: Kohout Michal doc. Ing. Ph.D.
Interchangeability : N110006
This subject contains the following additional online materials
Annotation -
Last update: Hladíková Jana (03.01.2018)
The basic aim of this course is to gain knowledge about principles and practical use of spectroscopic method in the field of organic chemistry.
Aim of the course -
Last update: Hladíková Jana (03.01.2018)

Students will be able to :

understand basic principles of spectroscopic methods in organic chemistry

use NMR, IR , UV-VIS and MS spectra in structure analysis of organic compounds

Literature -
Last update: Hladíková Jana (03.01.2018)

R: Böhm S., Smrčková S.: Strukturní analýza organických sloučenin, VŠCHT, 1995. 8070802359

A: Williams D.H., Fleming I.: Spectroscopic methods in organic chemistry. 5. vydání. DH Williams & I Fleming. 9780077091477

Learning resources -
Last update: Hladíková Jana (03.01.2018)

Teaching support to lectures at the lecturer

Syllabus -
Last update: Hladíková Jana (03.01.2018)

1. Overview of molecular spectroscopy methods, base conception and principles

2. NMR, base info, main conceptions, range of application

3. 1H NMR in organic structure analysis

4. 13C NMR in organic structure analysis

5. Special techniques of NMR

6. 2D NMR - COSY, HETCOR

7. Infrared spectroscopy, base conception and principles

8. Characteristic vibrations and „finger print“ region

9. Applications in structure analysis

10. UV-VIS spectroscopy, base conception and principles

11. Practical applications in structure analysis

12. Mass spectra, fundamental of method, experimental arrangement

13. Ionisation technique, separation techniques, basic types of fragmentation

14. Application in structure analysis of organic compounds

Registration requirements -
Last update: Kundrát Ondřej Ing. Ph.D. (03.01.2018)

Organic Chemistry II or Organic Chemistry B, Physics

Course completion requirements -
Last update: Kundrát Ondřej Ing. Ph.D. (15.02.2018)

The subject is concluded by an exam, which consists of a practical part involving the determination of the structure of a molecule from spectra and a theoretical part.

Teaching methods
Activity Credits Hours
Účast na přednáškách 1 28
Příprava na přednášky, semináře, laboratoře, exkurzi nebo praxi 1 28
Příprava na zkoušku a její absolvování 1,5 42
Účast na seminářích 0,5 14
4 / 4 112 / 112
 
VŠCHT Praha