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Last update: Fialová Jana (18.12.2017)
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Last update: MORAVCOJ (01.02.2018)
Students will be able: to understand physical-chemical principles of isolation and identification of organic compounds to optimize basic processes for isolation of organic compounds from a mixture to identify organic compounds and interpret the results at a basic level to assess product purity from spectral data to decide between alternative isolation and separation methods |
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Last update: Fialová Jana (18.12.2017)
R: Fogler H.S., Elements of Reaction Engineering, Prentice, Hall, New Jersey,2000,0130473944 |
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Last update: Fialová Jana (18.12.2017)
Lecture notes |
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Last update: MORAVCOJ (01.02.2018)
1. Introduction, problem formulation, up and down stream processes, economical aspects, operation safety 2. Features of organic and inorganic compounds suitable for separation, economical aspects, operation safety 3. Overview of down stream processes, fundamental characteristics, alternative methods 4. Removing solid particles: filtration, microfiltration, ultrafiltration, treatment of suspension before filtration, centrifugation 5. Extraction (batch), optimization of distribution coefficient, pH, ion pairs formation 6. Adsorption: solid-liquid batch, adsorption isotherms, mass balance 7. Sorbents, overview and applications, mobile phase selection 8. Chromatography: theoretical description of a phenomenon, instrumentation, analytical and preparative arrangement 9. Chromatography: elution liquid chromatography, Gauss equation, yield and purity of fractions 10. Electro migration methods, analytical and preparative, gas chromatography, stationery phases, instrumentation 11. Destillation, crystallization, drying, precipitation 12. UV, VIS, X-ray, and IR spectrometry, applications 13. Nuclear magnetic resonance, principle, applications 14. Mass spectrometry, principle, applications
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Last update: Fialová Jana (18.12.2017)
Organic chemistry I Mathematics I |
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Last update: MORAVCOJ (27.02.2018)
Napsání zápočtového testu nad 50 % Ústní zkouška |