SubjectsSubjects(version: 922)
Course, academic year 2021/2022
Special analytical methods for pharmaceuticals - B402009
Title: Speciální analytické metody pro léčiva
Guaranteed by: Department of Analytical Chemistry (402)
Faculty: Faculty of Chemical Engineering
Actual: from 2021
Semester: winter
Points: winter s.:3
E-Credits: winter s.:3
Examination process: winter s.:
Hours per week, examination: winter s.:2/0, Ex [HT]
Capacity: 12 / unknown (unknown)
Min. number of students: unlimited
Language: Czech
Teaching methods: full-time
For type: Bachelor's
Additional information:
Note: course can be enrolled in outside the study plan
enabled for web enrollment
Guarantor: Řezanka Pavel doc. RNDr. Ing. Ph.D.
Interchangeability : N402061
This subject contains the following additional online materials
Annotation -
Last update: Kubová Petra Ing. (16.01.2018)
The lectures are focused on drug analysis.
Aim of the course -
Last update: Kubová Petra Ing. (16.01.2018)

Students will be able to:

be well informed about analytical methods used for drug analysis

solve problems of drug analysis

evaluate and interpret data obtained by drug analysis.

Literature -
Last update: Kubová Petra Ing. (16.01.2018)

A: Zheng J. (Editor), Formulation and Analytical Development for Low-Dose Oral Drug Products, Wiley, 2009, ISBN: 978-0-470-05609-7.

A: Gunzler H., Williams A. (Editors), Handbook of Analytical Techniques, 2 Volume Set, Wiley, 2001, ISBN: 978-3-527-30165-2.

A: Gough T. A., The Analysis of Drugs of Abuse, Wiley, 1999, ISBN: 978-0-471-92267-4.

Learning resources -
Last update: Kubová Petra Ing. (16.01.2018)

Teaching methods -
Last update: Kubová Petra Ing. (16.01.2018)

Every week there is a two hour lecture.

Requirements to the exam -
Last update: Kubová Petra Ing. (16.01.2018)

1. The examination is written and takes 60 min.

2. Students, who study in Czech, pass examination in Czech. Students, who study in English, pass Examination in English.

3. Student is duty to present Index with written credit during the examination, otherwise it is impossible to continue in Examination.

4. The students sign in for the examination using SIS and it is duty of student to sign in for the term listed here. Signing off is possible up to date listed in SIS. Later it is possible only by request to secretary of department and only because of serious reasons. The examination is classified "F" when the student is absent and not signed off.

5. The assistant can allow writing examination when student arrives late. The missed time is not compensated.

6. It is not allowed to leave room during examination. It is not allowed to use forbidden materials and tools including telecommunication tools.

7. The place and the time will be announced during the examination. The examiner assign where and when will be possible to see checked examination test. If the student is not present in this time he or she resigns for any complain and agree with results. When student do not agree with classification of any of parts of test, the examiner will provide one, exceptionally more, additional question which will be answered in written form. According to result of these additional questions the examiner can change overall classification of examination by one step up or down.

8. Student can use only two reparative terms.

Syllabus -
Last update: Kubová Petra Ing. (16.01.2018)

1. Introduction to the Solid State

2. Thermal Analysis I

3. Thermal Analysis II

4. Thermal Analysis III

5. Isothermal Analysis

6. Calorimetric Methods

7. Surface Analysis I

8. Surface Analysis II

9. Particulate Analysis I

10. Particulate Analysis II

11. Computational Polymorph Prediction

12. Patenting of Inventions Relating to Polymorphs

13. A ‘Roadmap’ to Solid Form Selection

14. Drug evaluation

Entry requirements -
Last update: Kubová Petra Ing. (16.01.2018)

The students need to know analytical chemistry on the level of Analytical chemistry I.

Registration requirements -
Last update: Kubová Petra Ing. (16.01.2018)

The students need to know analytical chemistry on the level of Analytical chemistry I.

Teaching methods
Activity Credits Hours
Účast na přednáškách 1 28
Příprava na přednášky, semináře, laboratoře, exkurzi nebo praxi 1 28
Příprava na zkoušku a její absolvování 1 28
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