SubjectsSubjects(version: 950)
Course, academic year 2021/2022
Structural Crystallography - M108004
Title: Strukturní krystalografie
Guaranteed by: Department of Solid State Chemistry (108)
Faculty: Faculty of Chemical Technology
Actual: from 2019
Semester: winter
Points: winter s.:3
E-Credits: winter s.:3
Examination process: winter s.:
Hours per week, examination: winter s.:2/0, Ex [HT]
Capacity: 10 / unknown (unknown)
Min. number of students: unlimited
Language: Czech
Teaching methods: full-time
Teaching methods: full-time
For type: Master's (post-Bachelor)
Note: course can be enrolled in outside the study plan
enabled for web enrollment
Guarantor: Hušák Michal doc. Dr. Ing.
Interchangeability : N108011
Annotation -
Last update: Fialová Jana (04.01.2018)
The aim of the course is to teach students how to obtain information about the complete structure of investigated compound using diffraction methods. The course is suitable for pharmacists, organic chemists but also inorganic chemists who need to analyse crystalline products.
Aim of the course -
Last update: Fialová Jana (04.01.2018)

Students will be able to:

Utilize the methodology of X-ray diffraction analysis in the form of their own experiments.

Interpret the results of X-ray diffraction analysis from databases and literature.

Propose appropriate analytical methods for the solution associated with the solid state phase's analysis.

Literature -
Last update: Fialová Jana (04.01.2018)

R:Kratochvíl B., Chemie a fyzika pevných látek I, VŠCHT Praha, 1994, 8070801964

R:Kratochvíl B., Jenšovský L., Úvod do krystalochemie, SNTL Praha, 1987, 0460887

Learning resources -
Last update: Fialová Jana (04.01.2018)

R:Lectures in power-point form (actual version available by the lecturer)

Teaching methods - Czech
Last update: Fialová Jana (04.01.2018)

28 hodin přednášek

Requirements to the exam - Czech
Last update: Fialová Jana (04.01.2018)

Účast na přednáškách.

Syllabus -
Last update: Fialová Jana (04.01.2018)

1. Crystal structure. Space groups, application, matrix representation.

2. Types of radiation used for crystallographic studies and their characteristics.

3. Sources of radiation for crystallographic studies.

4. Bragg equation, Evald construction.

5. Different arrangement of diffraction experiments, in terms of radiation used and sample type.

6. Atomic scattering factor, structure factor.

7. Measuring on the four-circle diffractometer.

8. Correction's of diffraction data.

9. Methods for solving the phase problem.

10. Structure refinement from the diffraction data.

11. Specific problems of biological macromolecules structures solution.

12. Solution of crystal structures from powder diffraction data. Rietveld method.

13. Methods for solving crystal structures based on electron microscopy.

14. Databases of crystallographic data.

Registration requirements -
Last update: Fialová Jana (04.01.2018)

Chemistry and Physics of Solids

Mathematics I

Course completion requirements - Czech
Last update: Hušák Michal doc. Dr. Ing. (16.02.2018)

Absolvování ústní zkoušky.

Teaching methods
Activity Credits Hours
Konzultace s vyučujícími 0.5 14
Účast na přednáškách 1 28
Příprava na přednášky, semináře, laboratoře, exkurzi nebo praxi 0.5 14
Příprava na zkoušku a její absolvování 1 28
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