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Last update: Kubová Petra Ing. (15.01.2018)
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Last update: Kubová Petra Ing. (15.01.2018)
Students will be able to:
perform search in the databases ICSD and CSD; calculate theoretical powder pattren from structural data(X,Y,Z atomic positons); perform Rietveld analysis for quantitative phase determination, amorphous content determination, crystallite size determination. |
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Last update: Kubová Petra Ing. (15.01.2018)
A: Special manuscripts to the topics |
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Last update: Čejka Jan Ing. Ph.D. (20.02.2018)
https://serc.carleton.edu/research_education/geochemsheets/techniques/XRD.html |
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Last update: Kubová Petra Ing. (15.01.2018)
Students choose one of exercises mentioned below to solving:
1. Calculation of theoretical powder pattern from structural data(X,Y,Z atomic positons) using PDF4+ card or *.CIF file from ICSD or CSD - performed in program HighScore Plus 3.0. 2. Application of Rietveld analysis for quantitative phase determination 3. Application of Rietveld analysis for amorphous content determination. 4. Crystallite size determination, Hall-Williamson graph. 5. Search-match in Inorganic Crystal Structure Database(ICSD) - inorganic compounds, getting structural data as *.CIF file. 6. Search-match in Cambridge Structural Database(CSD) - organic compounds, getting structural data as *.CIF file. 7. Graphical presentation of structure - programs Mercury and Ortep.
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Last update: Maixner Jaroslav RNDr. CSc. (20.02.2018)
Credit – evaluation of powder pattern with program HighScore Plus 3.0 Examination – written part - test, Rietveld quantitative analysis with program HighScore Plus 3.0, oral part |
Teaching methods | ||||
Activity | Credits | Hours | ||
Účast na přednáškách | 1 | 28 | ||
Příprava na přednášky, semináře, laboratoře, exkurzi nebo praxi | 1 | 28 | ||
Příprava na zkoušku a její absolvování | 1.5 | 42 | ||
Účast na seminářích | 0.5 | 14 | ||
4 / 4 | 112 / 112 |