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Last update: Pátková Vlasta (17.01.2018)
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Last update: Pátková Vlasta (17.01.2018)
Students will be able to: Understand the wide range of separation and spectroscopy methods for chemical analysis of different types of complex hydrocarbon samples. Propose a rational treatment process and final analysis of real fuel materials, fractions and products. Identify the major components of complex hydrocarbon samples. |
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Last update: Staš Martin Ing. Ph.D. (08.11.2022)
S. Ch. Hsu: Analytical Advances for Hydrocarbon Research, Springer-Science+Business Media, LLC 2003. ISBN: 978-1-4613-4840-5. J. G. Speight: Handbook of Petroleum Product Analysis; John Wiley & Sons: New Jersey (USA), 2002. J. Mostecky, S. Hála, M. Kuraš, M. Popl: Analysis of hydrocarbon raw materials, STNL/ALFA 1984. S. Hála, M. Kuraš, M. Popl: Analysis of Complex Hydrocarbon Mixtures; Elsevier: Amsterdam, 1981. M. Staš, M. Auersvald, L. Kejla, D. Vrtiška, J. Kroufek, D. Kubička: Quantitative Analysis of Pyrolysis Bio-oils: A Review. Trends in Analytical Chemistry 2020, 126, 115857. M. Staš, M. Auersvald, P. Vozka: Two-Dimensional Gas Chromatography Characterization of Pyrolysis Bio-oils: A Review. Energy & Fuels 2021, 35 (10), 8541–8557. M. Staš, J. Chudoba, D. Kubička, J. Blažek, M. Pospíšil: Petroleomic Characterization of Pyrolysis Bio-oils: A Review. Energy & Fuels 2017, 31 (10), 10283-10299.
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Last update: Staš Martin Ing. Ph.D. (08.11.2022)
M. Pospíšil, M. Staš: Special analysis of fuels, internal educational presentations, available via e-learning. M. Staš et al.: Hydrocarbon Analysis and Environment - electronic studying text, available via e-learning. |
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Last update: Pátková Vlasta (17.01.2018)
1. Introduction - classification of analytical methods, qualitative and quantitative analysis. 2. Separation methods in the analysis (distillation, absorption, adsorption, extraction) - instrumentation, sample preparation and actual implementation, evaluation, examples 3. Chromatography - introduction, classification, basic terminology, qualitative and quantitative analysis, application depending on the type of sample. 4. Gas chromatography - columns, detectors and injectors, common configurations, preparation of samples for analysis, GC applications. 5. Liquid chromatography (HPLC, LSC, GPC) - operating conditions, instrumentation, LC detectors, sample preparation, LC applications. 6. UV, fluorimetry - principles, instrumentation, sample preparation, evaluation - quality/quantity, applications. 7. FTIR - principles, instrumentation, sample preparation, evaluation - quality/quantity, applications. 8. MS, NMR - principles, instrumentation, sample preparation, evaluation, applications. 9. Determination of metals and elements (AAS, AES, ICP, X-ray) - principles, advantages/disadvantages, instrumentation, sample preparation, evaluation, applications. 10. Thermal methods (DTA, TGA, DSC, pyrolysis) - principles, advantages/disadvantages, instrumentation, evaluation, applications. 11. Quality assessment of gaseous fuels - an overview of monitored parameters, choice of appropriate procedures for the sampling and analysis. 12. Quality assessment of petroleum fractions and products - an overview of monitored parameters, choice of appropriate analytical procedures. 13. Quality assessment of solid fuels and products of their processing - an overview of the parameters, choice of appropriate procedures for sampling and analysis. 14. Special trace analysis of selected pollutants (PAHs, PCBs, aldehydes, phenols, volatile organic compounds, sulfur-containing substances, organometallic compounds) - sampling, sample preparation, final analysis. |
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Last update: Pátková Vlasta (17.01.2018)
Organic Chemistry I, Analytical Chemistry I |
Teaching methods | ||||
Activity | Credits | Hours | ||
Účast na přednáškách | 1,5 | 42 | ||
Příprava na zkoušku a její absolvování | 3,5 | 98 | ||
5 / 5 | 140 / 140 |