SubjectsSubjects(version: 861)
Course, academic year 2019/2020
  
Field Portable Analysis - M240019
Title: Terénní a mobilní analýza
Guaranteed by: Department of Environmental Chemistry (240)
Actual: from 2019
Semester: winter
Points: winter s.:4
E-Credits: winter s.:4
Examination process: winter s.:
Hours per week, examination: winter s.:2/1 C+Ex [hours/week]
Capacity: unknown / unknown (unknown)
Min. number of students: unlimited
Language: Czech
Teaching methods: full-time
Level:  
For type: Master's (post-Bachelor)
Additional information: https://uchop.vscht.cz/predmety/portables
Note: course can be enrolled in outside the study plan
enabled for web enrollment
Guarantor: Hendrych Jiří Ing. Ph.D.
This subject contains the following additional online materials
Annotation -
Last update: Martinec Marek Mgr. Ing. Ph.D. (25.01.2018)
Students will learn the principles of portable analytical methods and their use for analyzes in the field. They learn to choose a suitable analytical method for specific types of samples, learn the principles of correct sampling and in-situ analysis. Students will also acquire practical skills with field analyzers and will be familiar with the basics of safety at work with portable analytic devices.
Aim of the course -
Last update: Martinec Marek Mgr. Ing. Ph.D. (25.01.2018)

Students will be able to:

Orient in portable instrumental analytical methods.

Know basic principles of spectral methods and interpretation of acquired spectra.

Evaluate the quality and reliability of analytical results.

Know the principles of sampling for field analysis and transport to the laboratory.

Solve specific problems of real sample analysis.

Know the basic principles of work safety with portable analytical instruments and the basics of first aid.

Literature -
Last update: Martinec Marek Mgr. Ing. Ph.D. (25.01.2018)

R:KEALEY, D. a P. J. HAINES. Analytical chemistry. Oxford: BIOS, 2002. Instant notes series. ISBN 1-85996-189-4.

R:ROBINSON, James W., Eileen M. Skelly FRAME a George M. FRAME. Undergraduate instrumental analysis. 6th ed. /. New York: M. Dekker, c2005. ISBN 0-8247-5359-3.

R:ROUESSAC, Francis. a Annick. ROUESSAC. Chemical analysis: modern instrumentation methods and techniques. 2nd ed. Chichester: John Wiley, 2007. ISBN 978-0-470-85903-2.

Learning resources -
Last update: Martinec Marek Mgr. Ing. Ph.D. (25.01.2018)

https://uchop.vscht.cz/predmety/portables

Syllabus -
Last update: Martinec Marek Mgr. Ing. Ph.D. (29.01.2018)

1. Use of portable analyzers in the field

2. Mobile analysis of hazardous gaseous and volatile substances (PID, FID, ...), CHMI (AIM, MIM, ISKO)

3. Multiparametric probes (pH, ORP, conductivity, DO, ISE, optical and electrochemical electrodes)

4. UV-VIS spectrophotometers, field analysis of the composition of liquids

5. Raman spectrometry and portable Raman spectrometers

6. Infrared spectrometry and portable FT-IR and NIR spectrometers

7. Radioactivity and Geiger-Müller counters

8. Portable gamma spectrometers and portable XRF spectrometers

9. Portable GC-MS detectors, gas chromatography and detectors

10. Sampling and adjustment of samples for field measurements and sample transport

11. Field analysis of gases, liquids and solids

12. Field analysis of unknown and dangerous substances, analysis of valuable items and artwork

13. Safety at work with portable analytical devices

14. First aid in the field

Entry requirements -
Last update: Martinec Marek Mgr. Ing. Ph.D. (25.01.2018)

Passing Analytical Chemistry I and II or Analytical Chemistry A and B

Registration requirements -
Last update: Martinec Marek Mgr. Ing. Ph.D. (25.01.2018)

General and inorganic chemistry

Organic chemistry

Physics

Physical chemistry

Course completion requirements -
Last update: Martinec Marek Mgr. Ing. Ph.D. (29.01.2018)

In order to successfully complete this course, students have to obtain a credit and pass the final exam. To obtain credit, students have to actively participate on all exercises. The credit is obligatory condition for admission to the final exam. The final exam will consist of two parts - a written test and an oral exam.

Teaching methods
Activity Credits Hours
Účast na přednáškách 0,5 14
Příprava na zkoušku a její absolvování 2 56
Účast na seminářích 1,5 42
4 / 4 112 / 112
Coursework assessment
Form Significance
Examination test 50
Continuous assessment of study performance and course -credit tests 25
Oral examination 25

 
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