SubjectsSubjects(version: 954)
Course, academic year 2019/2020
Isolation and Separation of Molecules - M342005
Title: Izolace a separace molekul
Guaranteed by: Department of Chemistry of Natural Compounds (342)
Faculty: Faculty of Food and Biochemical Technology
Actual: from 2019
Semester: winter
Points: winter s.:4
E-Credits: winter s.:4
Examination process: winter s.:
Hours per week, examination: winter s.:2/1, C+Ex [HT]
Capacity: 24 / unlimited (unknown)
Min. number of students: unlimited
State of the course: taught
Language: Czech
Teaching methods: full-time
Teaching methods: full-time
Note: course can be enrolled in outside the study plan
enabled for web enrollment
Guarantor: Prokudina Elena Ing. Ph.D.
Examination dates   Schedule   
This subject contains the following additional online materials
Annotation -
The course covers selected technological procedures from the point of view of a selection from alternative methods and possibilities how to affect efficiency and capacity of these operations. It emphasizes user view of unit technological operations.
Last update: Kubová Petra (19.12.2017)
Aim of the course -

Students will be able to:

Design a suitable isolation method

Optimize efficiency and capacity of an isolation method

Select a suitable separation method

Have an overview of technological aspects of discussed isolation and separation methods

Last update: Kubová Petra (19.12.2017)
Literature -

R: Fogler H.S.: Elements of Reaction Engineering,Prentice,Hall,New Jersey,2000,0130473944

Last update: Kubová Petra (19.12.2017)
Learning resources -

Lecture notes

Last update: Kubová Petra (19.12.2017)
Syllabus -

1. Introduction, formulation of a problem, process characterization

2. Separation of solid particles: filtration, microfiltration, ultrafiltration, centrifugation

3. Methods of suspension adjustments, effect of electrolytes, temperature, ionic strength, sorbents

4. Extraction and adsorption, comparison of basic parameters (equilibrium, interruptibility, efficiency, capacity, selectivity

5. Batch extraction, continuous extraction, Craig extraction, effect of pH, ion pairs formation

6. Batch adsorption, continuous adsorption, adsorption on a solid bed (approximation)

7. Chromatography: sorbents, instrumentation, implementation, mobile phase selection

8. Chromatography: Gauss equation, Poisson distribution, yield, and fraction purity

9. Chromatography: up-scaling

10. Precipitation, electrophoresis

11. Electro dialysis, isoelectric focusation

12. Crystallization, drying

13. Economic aspects of alternative methods, solvent regeneration, operation safety

14. Methods of choice

Last update: Kubová Petra (19.12.2017)
Registration requirements -

Organic chemistry

Mathematics I

General and inorganic chemistry

Last update: Kubová Petra (19.12.2017)
Course completion requirements - Czech

Absolvování zápočtového testu minimálně na 50 %.

Ústní zkouška.

Last update: MORAVCOJ (23.02.2018)
Coursework assessment
Form Significance
Regular attendance 20
Continuous assessment of study performance and course -credit tests 30
Oral examination 50