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The lectures are focused on separation techniques. Besides well known techniques less common methods that have great separation potencial are also discussed.
Last update: Řezanka Pavel (31.01.2018)
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Předmět je zakončen písemnou a ústní zkouškou. Pro udělení zápočtu student musí student ze zápočtového testu získat alespoň 50% bodů. Last update: Řezanka Pavel (31.01.2018)
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R: Analytická separace látek - kniha, J. Churáček; SNTL, 1990. R: High Performance Capillary Electrophoresis - firemní příručka, D.N. Heiger, Hewlett-Packard, 1992. R: Basic Gas Chromatography - kniha, H.M. McNair and J.M. Miller, Wiley, 2009, ISBN: 978-0-470-43954-8. R: Practical High-Performance Liquid Chromatography - kniha, V.R. Meyer, Wiley, 2010, ISBN:978-0-470-68218-0. R: Introduction to Mass Spectrometry - kniha, J.T. Watson and O.D. Sparkman, Wiley, 2007, ISBN: 978-0-470-51634-8. A: Mass Spectrometry-A Textbook - kniha, J.H. Gross, 2004, Springer, ISBN: 3-540-40739-1. A: Introduction to Modern Liquid Chromatography - kniha, L.R. Snyder, J.J. Kirkland and J.W. Dolan, Wiley, 2010, ISBN:978-0-470-16754-0. A: Gas Chromatography and Mass Spectrometry-A Practical Guide - kniha, O.D. Sparkman, Z.E. Penton, and F.G. Kitson, 2011, Elsevier, ISBN:978-0-12-373628-4. A: Practical HPLC Method Development - kniha, L.R. Snyder, J.J. Kirkland, J.L. Glajch; Wiley, 1997, ISBN:0-471-00703-X. A: Chromatographic methods - kniha, A. Braithwaite, F.J. Smith; Blackie Academic & Proffessional, 1996, ISBN:0-7514-0158-7. A: Gas Chromatography - kniha, I.A. Fowlis; ACOL, Wiley, 1995, ISBN:0-471-95467-5. A: High Performance Liquid Chromatography - kniha, S. Lindsay; ACOL, Wiley, 1992, ISBN:0-471-93180-2. A: Separace látek - skripta, M. Popl, J. Kubát; SNTL, 1986. A: Chromatography Today - kniha, C.F. Poole, S.K. Poole; Elsevier, 1991, ISBN:0-444-88492-0. Last update: Pátková Vlasta (05.01.2018)
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Every week there is a two hour lecture and one hour seminar. Last update: Řezanka Pavel (31.01.2018)
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1. Gas chromatograophy - detailed theory, van Deemter plots.
2. Gas chromatograophy - current trends.
3. High-performance chromatography - detailed theory, kinetic plots.
4. High-performance chromatography - current trends
5. Ultrahigh-performance chromatography.
6. Electrophoresis.
7. Capillary electrophoresis.
8. Separation on chips and high-throughput techniques.
9. Solid phase extraction - current status.
10. Simulated moving bead technology.
11. Supercritical fluid chromatography.
12. Mass spectrometry - 1.
13. Mass spectrometry - 2.
14. Webinars - useful source of information. Last update: Sýkora David (19.01.2018)
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http://onlinelibrary.wiley.com/book/10.1002/9780470688427 Last update: Pátková Vlasta (05.01.2018)
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Students will be able to:
be well informed about separation methods
solve problems of real samples separations
evaluate and interpret data obtained by separation analysis. Last update: Pátková Vlasta (05.01.2018)
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The students need to know analytical chemistry on the level of Analytical chemistry I. Last update: Pátková Vlasta (05.01.2018)
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The students need to know analytical chemistry on the level of Analytical chemistry I. Last update: Pátková Vlasta (05.01.2018)
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| Teaching methods | ||||
| Activity | Credits | Hours | ||
| Konzultace s vyučujícími | 0.5 | 14 | ||
| Účast na přednáškách | 1 | 28 | ||
| Příprava na přednášky, semináře, laboratoře, exkurzi nebo praxi | 1 | 28 | ||
| Příprava na zkoušku a její absolvování | 1 | 28 | ||
| Účast na seminářích | 0.5 | 14 | ||
| 4 / 4 | 112 / 112 | |||