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Students will learn about laboratory safety, basic laboratory equipment and experimental procedures used in organic chemistry. Working on several simple organic syntheses, students will acquire the requisite skills for the preparation and characterization of organic compounds. Final grade is based not only on the performance in the laboratory, but also on the knowledge of simple calculations (stoichiometry and preparation of solutions) and the chemical principles of procedures carried out.
Last update: MARTINUT (02.08.2013)
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R: J. W. Zubrick, The Organic Chem Lab Survival Manual: A Student's Guide to Techniques, 5th Ed., Wiley 2001.0471387320 Last update: Cibulka Radek (05.02.2015)
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1. Laboratory safety and first aid instructions. 2. Laboratory rules, recordkeeping, protocols, essential calculations. 3. Basic laboratory equipment. 4. Building of reaction apparatuses. 5. Crystallization and filtration. 6. Organic solvents, extraction, drying, evaporation. 7. Stirring and heating under reflux. 8. One-step syntheses of various organic substances, isolation and identification of products. 9. Multi-step syntheses. 10. Operations under anhydrous conditions. 11. Distillation under ambient pressure. 12. Distillation under reduced pressure. 13. Melting point determination. 14. Gas chromatography. Last update: MARTINUT (02.08.2013)
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Laboratory instructions Last update: MARTINUT (02.08.2013)
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Students will be able to: work safely in organic laboratory carry out basic laboratory operations combine the theoretical knowledge with experimental results understand the system of organic synthesis - reaction planning, building a reaction apparatus, carrying out a reaction, isolation and characterization of products write laboratory protocols Last update: Cibulka Radek (19.08.2013)
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Organic chemistry I or Organic Chemistry A and Inorganic Chemistry: Laboratory I. Last update: Cibulka Radek (14.09.2016)
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Organic chemistry I or Organic Chemistry A and Inorganic Chemistry: Laboratory I. Last update: Cibulka Radek (14.09.2016)
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Teaching methods | ||||
Activity | Credits | Hours | ||
Účast v laboratořích (na exkurzi nebo praxi) | 2 | 56 | ||
Příprava na přednášky, semináře, laboratoře, exkurzi nebo praxi | 1 | 28 | ||
3 / 3 | 84 / 84 |
Coursework assessment | |
Form | Significance |
Regular attendance | 40 |
Report from individual projects | 30 |
Continuous assessment of study performance and course -credit tests | 30 |