SubjectsSubjects(version: 855)
Course, academic year 2019/2020
  
Organic Chemistry: Laboratory II - N110003
Title: Laboratoř organické chemie II
Guaranteed by: Department of Organic Chemistry (110)
Actual: from 2017
Semester: both
Points: 4
E-Credits: 4
Examination process:
Hours per week, examination: 0/4 MC [hours/week]
Capacity: winter:unknown / unknown (unknown)
summer:unknown / unknown (unknown)
Min. number of students: unlimited
Language: Czech
Teaching methods: full-time
Level:  
For type:  
Additional information: http://Do termínu laboratoří se musí studenti přihlásit prostřednictvím SIS jako na termín zkoušky z Laboratoří OCH II
Note: course can be enrolled in outside the study plan
enabled for web enrollment
you can enroll for the course in winter and in summer semester
Guarantor: Kozmík Václav Ing. CSc.
Pre-requisite : {x}, {x}
Interchangeability : N110003A
Is interchangeable with: N110003A
Annotation -
Last update: MARTINUT (02.08.2013)
Development of skills obtained in the preceding course, column chromatography and spectroscopical characterization of products.
Aim of the course -
Last update: Cibulka Radek prof. Ing. Ph.D. (19.08.2013)

Students will be able to:

combine the theoretical knowledge with experimental results

understand the system of organic synthesis - reaction planning, building a reaction apparatus, carrying out a reaction, isolation and characterization of products

write laboratory protocols

Literature -
Last update: Cibulka Radek prof. Ing. Ph.D. (28.08.2013)

R: Šilhánková a kol.: Laboratoř organické chemie, Vydavatelství VŠCHT, 2000, dotisk 2007, 8070803959

Learning resources -
Last update: MARTINUT (02.08.2013)

Laboratory instructions

Syllabus -
Last update: MARTINUT (02.08.2013)

1. Laboratory safety and first aid instructions.

2. One-step syntheses of various organic substances, isolation and identification of products.

3. Multi-step syntheses.

4. Operations under anhydrous conditions.

5. Operations on semimicroscale.

6. Organic solvents, extraction, drying, evaporation.

7. Crystallization and filtration.

8. Column chromatography.

9. Thin layer chromatography.

10. Distillation under ambient pressure.

11. Distillation under reduced pressure.

12. Melting point determination.

13. Gas chromatography.

14. NMR spectrometry.

Entry requirements -
Last update: MARTINUT (02.08.2013)

Organic chemistry: Laboratory I

Registration requirements -
Last update: MARTINUT (02.08.2013)

Organic chemistry: Laboratory I

Teaching methods
Activity Credits Hours
Účast v laboratořích (na exkurzi nebo praxi) 2 56
Příprava na přednášky, semináře, laboratoře, exkurzi nebo praxi 1 28
Práce na individuálním projektu 1 28
4 / 4 112 / 112
Coursework assessment
Form Significance
Regular attendance 40
Report from individual projects 30
Continuous assessment of study performance and course -credit tests 30

 
VŠCHT Praha