SubjectsSubjects(version: 899)
Course, academic year 2021/2022
  
Specialized Laboratory I - N112018
Title: Laboratoř oboru I
Guaranteed by: Department of Polymers (112)
Actual: from 2020
Semester: winter
Points: winter s.:7
E-Credits: winter s.:7
Examination process: winter s.:
Hours per week, examination: winter s.:0/10 MC [hours/week]
Capacity: unknown / unknown (unknown)
Min. number of students: unlimited
Language: Czech
Teaching methods: full-time
Level:  
Is provided by: M112011
For type:  
Guarantor: Malinová Lenka Ing. Ph.D.
Is interchangeable with: M112011
Examination dates   Schedule   
Annotation -
Last update: Brožek Jiří prof. Ing. CSc. (10.07.2012)
Laboratory practise is focused on preparation of polymers by emulsion, suspension, block a solution polymerizations using various radical and ionic initiators, kinetic of polymerization reactions, determination of basic physical and chemical characteristics of prepared polymers and adopting of basic methods in identification of polymer samples.
Aim of the course -
Last update: Fialová Jana (15.08.2013)

Students will be able to: (i) prepare polymers with different procedures, (ii) characterize prepared polymers, (iii) evaluate kinetic of polymerization and (iv) identify basic polymers.

Literature -
Last update: Brožek Jiří prof. Ing. CSc. (01.08.2013)

R: Maroušek V.: Návody pro laboratorní cvičení z makromolekulární chemie, VŠCHT Praha 1997; ISBN 80-7080-287-1

Learning resources -
Last update: Brožek Jiří prof. Ing. CSc. (01.08.2013)

Encyclopedia of Polymer Science and Technology, J. Wiley @ Sons (available at http://www.vscht.cz/pol/)

Requirements to the exam - Czech
Last update: Brožek Jiří prof. Ing. CSc. (25.02.2009)

Podmínkou získání zápočtu je absolvování všech vypsaných prací. V případě neúčasti na laboratorní práci se student domluví o její náhradě s vedoucím. Při celkovém hodnocení studenta se klade hlavní důraz na praktické dovednosti.

Syllabus -
Last update: Brožek Jiří prof. Ing. CSc. (14.11.2012)

1. Introduction, health and safety at work - entry training.

2. Coordination polymerization of ethylene.

3. Equilibrium polymerization.

4. Preparation of soft contact lenses.

5. Preparation of silicone rubber.

6. Anionic polymerization/Preparation of glycolide or L-lactide by depolymerization.

7. Copolymerization of styrene.

8. Preparation of soft lences

9. Kinetic of polyesterification.

10. Monitoring of polymerization by dilatometry.

11. Determination of viscosity-average molar mass.

12. Determination of number-average molar mass (titration method).

13. Identification of polymers.

14. Summary, examination test.

Entry requirements -
Last update: Brožek Jiří prof. Ing. CSc. (10.07.2012)

To pass examination from Macromolecular chemistry.

Registration requirements -
Last update: TAJ112 (15.08.2013)

Macromolecular Chemistry, Organic Chemistry I

Teaching methods
Activity Credits Hours
Konzultace s vyučujícími 0,5 14
Účast v laboratořích (na exkurzi nebo praxi) 4,5 126
Obhajoba individuálního projektu 0,5 14
Příprava na přednášky, semináře, laboratoře, exkurzi nebo praxi 1 28
Příprava na zkoušku a její absolvování 0,5 14
7 / 7 196 / 196
Coursework assessment
Form Significance
Report from individual projects 70
Continuous assessment of study performance and course -credit tests 30

 
VŠCHT Praha