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Last update: TAJ342 (01.10.2013)
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Last update: TAJ342 (01.10.2013)
Students will be able to: Optimize basic processes for isolation of organic compounds from a mixture Identify organic compounds and interpret the results at a basic level Assess product purity from spectral data Decide between alternative isolation and separation methods |
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Last update: TAJ342 (01.10.2013)
R: Fogler H.S., Elements of Reaction Engineering, Prentice, Hall, New Jersey,2000,0130473944 |
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Last update: TAJ342 (01.10.2013)
Lecture notes |
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Last update: TAJ342 (01.10.2013)
1. Introduction, problem formulation, process characterization, definition of starting conditions 2. Removing solid particles: filtration, microfiltration, ultrafiltration, treatment of suspension before filtration 3. Centrifugation (common centrifuges), comparison of filtration and centrifugation 4. Extraction (batch, counter-flow), modification of distribution coefficient, pH, ion pairs formation 5. Adsorption (batch, continuous) 6. Sorbents, overview and applications, mobile phase selection 7. Chromatography: theoretical description of a phenomenon, instrumentation, analytical and preparative arrangement 8. Chromatography: yield, purity 9. Electro migration methods 10. Economical aspects of alternative methods, solvent regeneration, operation safety 11. Physico-chemical methods of identification of organic compounds 12. UV, VIS, and IR spectrometry, applications 13. Nuclear magnetic resonance, principle, applications 14. Mass spectrometry, principle, applications |
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Last update: TAJ342 (01.10.2013)
Organic chemistry I Mathematics I |
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Last update: MORAVCOJ (21.11.2012)
Napsání zápočtového testu Ústní zkouška |
Teaching methods | ||||
Activity | Credits | Hours | ||
Účast na přednáškách | 1 | 28 | ||
Příprava na přednášky, semináře, laboratoře, exkurzi nebo praxi | 1 | 28 | ||
Příprava na zkoušku a její absolvování | 1.5 | 42 | ||
Účast na seminářích | 0.5 | 14 | ||
4 / 4 | 112 / 112 |
Coursework assessment | |
Form | Significance |
Regular attendance | 20 |
Continuous assessment of study performance and course -credit tests | 30 |
Oral examination | 50 |