SubjectsSubjects(version: 855)
Course, academic year 2019/2020
  
Analytical Chemistry: Laboratory I - N402003A
Title: Laboratoř analytické chemie I
Guaranteed by: Department of Analytical Chemistry (402)
Actual: from 2019
Semester: summer
Points: summer s.:4
E-Credits: summer s.:4
Examination process: summer s.:
Hours per week, examination: summer s.:0/5 MC [hours/week]
Capacity: unknown / unknown (unknown)
Min. number of students: unlimited
Language: Czech
Teaching methods: full-time
Level:  
For type:  
Additional information: http://www.vscht.cz/anl/lach1/
Note: course can be enrolled in outside the study plan
enabled for web enrollment
Guarantor: Vosmanská Magda Ing. CSc.
Interchangeability : N402003
Is interchangeable with: B402005, N402003
Examination dates   Schedule   
Annotation -
Last update: Vosmanská Magda Ing. CSc. (29.05.2019)
The laboratory training is focused on acquiring praxis in analytical laboratory. Students learn how to work in a clean, accurate and correct way. The spectrum of methods includes chemical analysis (1-2 works), electrochemical (2-3), spectrophotometric (2) and separation (1) methods. The Laboratory is followed by Laboratory of Analytical Chemistry II.
Aim of the course -
Last update: Vosmanská Magda Ing. CSc. (29.05.2019)

Students will be able to:

do basic laboratory analytical operations

manipulate with different types of electrodes

work with spectrophotometer and liquid chromatograph

evaluate the results of the measurements

Literature -
Last update: Vosmanská Magda Ing. CSc. (29.05.2019)

Manuals are availabe for download at https://uanlch.vscht.cz/studium/bakalarske/laboratore/lachi

Learning resources -
Last update: Vosmanská Magda Ing. CSc. (29.05.2019)

https://uanlch.vscht.cz/studium/bakalarske/laboratore/lachi

Requirements to the exam -
Last update: Vosmanská Magda Ing. CSc. (29.05.2019)

The every laboratory starts with 5-minute 6-question test, to prove that student read the manual and is able to work safely and purposefully. The 3 questions need to be answered correctly to be allowed to work. If not, the test is classified F. Every work is classified after delivering of report or not classified if report is not delivered or delivered late. If the report was delivered in time and was not classified, the protocol needs to be corrected, in such case contact your teaching assistant. The overall classification is the arithmetic average off all marks, including all F for unsuccessful tests. To obtain final mark, all practices need to be passed with maximum two F.

Syllabus -
Last update: Vosmanská Magda Ing. CSc. (29.05.2019)

1. Gravimetric and chelatometric determination of nickel

2. Determination of fluorides by ISE

3. Potentiometric measurement of pH

4. Coulometric determination of ascorbic acid

5. Spectrophotometric determination of iron with 1,10-fenanthroline

6. Liquid chromatography

7. IR spectroscopy

Entry requirements -
Last update: Vosmanská Magda Ing. CSc. (29.05.2019)

The previous experience from chemical laboratory of any kind is expected. The knowledge of MS Excel is essential for some of labs (charts, basic calculation, working with cell references).

Registration requirements -
Last update: Vosmanská Magda Ing. CSc. (29.05.2019)

No

Teaching methods
Activity Credits Hours
Účast v laboratořích (na exkurzi nebo praxi) 2,5 70
Příprava na přednášky, semináře, laboratoře, exkurzi nebo praxi 1,5 42
4 / 4 112 / 112
Coursework assessment
Form Significance
Regular attendance 30
Report from individual projects 50
Continuous assessment of study performance and course -credit tests 20

 
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