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The laboratory training is focused on acquiring praxis in analytical laboratory. Students learn how to work in a clean, accurate and correct way. The spectrum of methods includes chemical analysis (1-2 works), electrochemical (2-3), spectrophotometric (2) and separation (1) methods. The Laboratory is followed by Laboratory of Analytical Chemistry II.
Last update: Vosmanská Magda (29.05.2019)
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Students will be able to: do basic laboratory analytical operations manipulate with different types of electrodes work with spectrophotometer and liquid chromatograph evaluate the results of the measurements Last update: Vosmanská Magda (29.05.2019)
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Manuals are availabe for download at https://uanlch.vscht.cz/studium/bakalarske/laboratore/lachi Last update: Vosmanská Magda (29.05.2019)
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The every laboratory starts with 5-minute 6-question test, to prove that student read the manual and is able to work safely and purposefully. The 3 questions need to be answered correctly to be allowed to work. If not, the test is classified F. Every work is classified after delivering of report or not classified if report is not delivered or delivered late. If the report was delivered in time and was not classified, the protocol needs to be corrected, in such case contact your teaching assistant. The overall classification is the arithmetic average off all marks, including all F for unsuccessful tests. To obtain final mark, all practices need to be passed with maximum two F. Last update: Vosmanská Magda (29.05.2019)
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1. Gravimetric and chelatometric determination of nickel 2. Determination of fluorides by ISE 3. Potentiometric measurement of pH 4. Coulometric determination of ascorbic acid 5. Spectrophotometric determination of iron with 1,10-fenanthroline 6. Liquid chromatography 7. IR spectroscopy Last update: Vosmanská Magda (29.05.2019)
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https://uanlch.vscht.cz/studium/bakalarske/laboratore/lachi Last update: Vosmanská Magda (29.05.2019)
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The previous experience from chemical laboratory of any kind is expected. The knowledge of MS Excel is essential for some of labs (charts, basic calculation, working with cell references). Last update: Vosmanská Magda (29.05.2019)
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No Last update: Vosmanská Magda (29.05.2019)
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| Teaching methods | ||||
| Activity | Credits | Hours | ||
| Účast v laboratořích (na exkurzi nebo praxi) | 2.5 | 70 | ||
| Příprava na přednášky, semináře, laboratoře, exkurzi nebo praxi | 1.5 | 42 | ||
| 4 / 4 | 112 / 112 | |||
| Coursework assessment | |
| Form | Significance |
| Regular attendance | 30 |
| Report from individual projects | 50 |
| Continuous assessment of study performance and course -credit tests | 20 |