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Last update: Mestek Oto prof. Ing. CSc. (15.09.2013)
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Last update: Mestek Oto prof. Ing. CSc. (15.09.2013)
Students completing the course will acquire theoretical and practical knowledge of the methods of elemental analysis using optical spectroscopy (absorption, emission and fluorescence), X-ray spectrometry and mass spectrometry. They will be familiar with the various methods of sample preparation and problems of cleanness in trace laboratory. |
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Last update: Mestek Oto prof. Ing. CSc. (20.02.2018)
R: Cullen M.: Atomic Spectroscopy in Elemental Analysis, Blackwell, ISBN 1-84127-333-3 R: José A.C. Broekaert: Analytical Atomic Spectrometry with Flames and Plasmas, Wiley, ISBN 978-3-527-31282-5 Skripta (in Czech): Černohorský T., Jandera P.: Atomová spektroskopie, Univerzita Pardubice 1997. ISBN 80-7194-114-X R: Ebdon L., Evans E.H., Fisher A.S., Hill S.J.: An Introduction to Analytical Atomic Spectrometry. Willey 1998, ISBN 978-0-471-97418-5 |
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Last update: Mestek Oto prof. Ing. CSc. (03.09.2013)
http://web.vscht.cz/~koplikr/Atomov%c3%a1%20%20spektrometrie.pdf |
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Last update: Mestek Oto prof. Ing. CSc. (15.09.2013)
Passing labs and acknowledgement of protocols by assistant professor. An oral examination. Student can use only two reparative terms. |
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Last update: Mestek Oto prof. Ing. CSc. (10.04.2018)
1. Structure of atoms.
2. Interaction of electrons and electromagnetic radiation, width and intensity of spectral lines.
3. Fundamentals of optics, construction of monochromators and polychromators, construction of radiation detectors.
4. Atomic absorption spectrometry, basic instrumentation - radiation sources, atomizers.
5. Atomic absorption spectrometry: interference and background correction, signal optimization and processing.
6. Atomic absorption spectrometry: special techniques - hydride generation, mercury determination, electrodeposition.
7. Atomic fluorescence spectrometry.
8. Flame emission spectrometry, spectrometry with electric arc and spark excitation, rotating electrode spectroscopy, spectroscopy with glow discharge.
9. Inductively coupled and DC plasma optical emission spectrometry, LIBS
10. Inductively coupled plasma mass spectrometry: basic instrumentation - ion optics, ion filters and detectors.
11. Inductively coupled plasma mass spectrometry: interference and methods of their elimination; special techniques - laser ablation, analysis of nanoparticles, connection with electrothermal evaporation.
12. Hyphenated techniques in speciation analysis of trace elements.
13. X-ray fluorescence spectrometry.
14. Preparation of samples for elemental trace analysis, principles of work in a trace laboratory.
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Last update: Mestek Oto prof. Ing. CSc. (03.09.2013)
Basic knowledge of analytical chemistry |
Teaching methods | ||||
Activity | Credits | Hours | ||
Konzultace s vyučujícími | 0.5 | 14 | ||
Účast v laboratořích (na exkurzi nebo praxi) | 1 | 28 | ||
Účast na přednáškách | 1 | 28 | ||
Příprava na přednášky, semináře, laboratoře, exkurzi nebo praxi | 1 | 28 | ||
Příprava na zkoušku a její absolvování | 1.5 | 42 | ||
5 / 5 | 140 / 140 |
Coursework assessment | |
Form | Significance |
Report from individual projects | 50 |
Oral examination | 50 |