SubjectsSubjects(version: 855)
Course, academic year 2019/2020
  
Spectroscopic Methods - N403046
Title: Spektroskopické metody
Guaranteed by: Department of Physical Chemistry (403)
Actual: from 2013
Semester: winter
Points: winter s.:3
E-Credits: winter s.:3
Examination process: winter s.:
Hours per week, examination: winter s.:1/1 C+Ex [hours/week]
Capacity: unlimited / unlimited (unknown)
Min. number of students: unlimited
Language: Czech
Teaching methods: full-time
Level:  
For type:  
Guarantor: Tkadlecová Marcela Ing. CSc.
Annotation -
Last update: TAJ403 (13.12.2013)
The crux of this subject consists in understanding the relation between the physical basis of individual spectroscopic method or technique and their application for study of the physical-chemical properties of substances. The accent will be put on the fact that the results of individual methods are complementary and confirm each other. Interpretation of spectra will be beside the identification of compounds aimed at the study of intermolecular interactions and supramolecular structures. The description of the instrumentation will be limited to basic facts on which the applications are based.
Aim of the course -
Last update: TAJ403 (13.12.2013)

Students will able to:

Understand the physical principles of spectroscopic methods

Apply these physical principles to the selection of methods which are appropriate for the study of the given properties of specific types of compounds

Interpret the results of measurements for individual methods

Combine the results of individual methods

Be familiar with basic instrumentation of methods with respect to resulting applications

Literature -
Last update: TAJ403 (10.09.2013)

R: Atkins P.W., de Paula J., Physical Chemistry, Oxford University Press, 2010, 9780199543373

A: Gauglitz G., Handbook of Spectroscopy,John Wiley & Sons, 2006, 3527297820

Learning resources -
Last update: TAJ403 (10.09.2013)

http://e-knihovna.vscht.cz/admin/default.aspx?page=1&ii=&td=&rok=&lokace=&v=1&p=9&kat=28&stav=*&new=*&od=&do=&rev=&starting=&autor=&nazev=Handbook+of+Spectroscopy

Syllabus -
Last update: TAJ403 (10.09.2013)

1. Introduction, basic concepts, basic principles

2. X-ray fluorescence analysis, photoelectron spectroscopy, Auger spectrosopy

3. Atomic absorption spectrometry, Atomic emission spectrometry

4. UV-VIS spectrosopy, FIA, nephelometry, turbidimetry

5. Luminiscence methods

6. Infrared spectrometry - basic principle, instrumentation and examples of applications

7. Interpretation of IR spectra

8. Raman spectrometry, rotational spectrometry

9. NMR- basic principle, instrumentation and examples of applications

10. Interpretation of NMR spectra

11. ss NMR, basic principle, instrumentation and examples of applications

12. Mass spectrometry, combined techniques

13. Interpretation of mass spectra

14. Chiroptical methods - optical activity, ECD, VCD and ROA, possibilities of NMR for study of optically active compounds

Registration requirements -
Last update: TAJ403 (10.09.2013)

Physical chemistry I

Teaching methods
Activity Credits Hours
Účast na přednáškách 0,5 14
Příprava na přednášky, semináře, laboratoře, exkurzi nebo praxi 1 28
Příprava na zkoušku a její absolvování 1 28
Účast na seminářích 0,5 14
3 / 3 84 / 84
Coursework assessment
Form Significance
Regular attendance 20
Examination test 40
Oral examination 40

 
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