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Last update: Merna Jan prof. Ing. Ph.D. (08.06.2018)
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Last update: Merna Jan prof. Ing. Ph.D. (08.06.2018)
Student will be able: To describe principle of selected analytical methods Choose a proper characterization method Assess the quality of information obtained by alternative methods |
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Last update: Merna Jan prof. Ing. Ph.D. (08.06.2018)
R: Podzimek, S., Light Scattering, Size Exclusion Chromatography and Asymmetric Flow Field Flow Fractionation. Wiley: 2011; ISBN 978-0-470-38617-0 R: Pethrick R.A., Dawkins J.V., Modern Techniques for Polymer Characterisation, John Wiley and Sons, 1999; ISBN 0-471-96097-7 A: Striegel, A. M.; Yau, W. W.; Kirkland, J. J.; Bly, D. D., Modern Size-Exclusion Liquid Chromatography: Practice of Gel Permeation and Gel Filtration Chromatography. Wiley: 2009, ISBN 978-0-471-20172-4 |
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Last update: Merna Jan prof. Ing. Ph.D. (08.06.2018)
Encyclopedia of Polymer Science and Technology, J. Wiley&Sons available from http://pol.vscht.cz/ |
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Last update: Merna Jan prof. Ing. Ph.D. (08.06.2018)
Lectures |
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Last update: Merna Jan prof. Ing. Ph.D. (08.06.2018)
The subject specifically focuses on the following topics: 1.Size exclusion chromatography of polymers, history, principles, mechanism, relative calibration, universal calibration 2.Size exclusion chromatography with multiple detection, LS, viscometer 3.Practical aspects of SEC analysis, copolymers analysis 4.Interaction chromatography (chromatography under critical conditions, adsorption barriers, IC with thermal and solvent gradient) 5.Polymer fractionation (FFF, TREF, CRYSTAF) 6.Mass spectroscopy of polymers (ESI, MALDI-TOF) 7.Pyrolysis chromatography, SPE 8.NMR of polymers (liquid and solid phase) 9.Methods for the characterization of thermal methods of polymers (DSC, DMA, TGA+MS/IR) 10.Methods of study of polymer surfaces (EM, AFM) |
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Last update: Merna Jan prof. Ing. Ph.D. (08.06.2018)
Macromolecular chemistry |
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Last update: Merna Jan prof. Ing. Ph.D. (08.06.2018)
Oral exam |