SubjectsSubjects(version: 865)
Course, academic year 2019/2020
  
Experimental Methods of Obtaining of Thermodynamic data of Solids - P126005
Title: Experimentální metody získávání termodynamických dat pevných látek
Guaranteed by: Department of Solid State Engineering (126)
Actual: from 2019
Semester: both
Points: 0
E-Credits: 0
Examination process:
Hours per week, examination: 2/1 other [hours/week]
Capacity: winter:unlimited / unlimited (unknown)
summer:unknown / unknown (unknown)
Min. number of students: unlimited
Language: Czech
Teaching methods: full-time
Level:  
For type: doctoral
Note: you can enroll for the course in winter and in summer semester
Guarantor: Leitner Jindřich prof. Ing. DrSc.
Sedmidubský David prof. Dr. Ing.
Z//Is interchangeable with: AP126005
Annotation -
Last update: Leitner Jindřich prof. Ing. DrSc. (25.06.2018)
The aim of this course is to introduce students to experimental determination of thermodynamic properties of solids.
Aim of the course -
Last update: Leitner Jindřich prof. Ing. DrSc. (25.06.2018)

Students will be able to:

Choose appropriate experimental methods for determination of the selected thermodynamic properties of solids.

Process and interpret experimental data.

To actively use selected experimental techniques.

Literature -
Last update: Leitner Jindřich prof. Ing. DrSc. (14.09.2018)

R: Kubaschewski O., Alcock C.B., Spencer P.J.: Materials Thermochemistry, 6th edition (512 pp). Pergamon (1993), ISBN-13: 978-0080418896

A: Sarge C.M., Höhne G.W.H., Hemminger W.: Calorimetry: Fundamentals, Instrumentation and Applications (304 pp). Wiley-VCH (2014), ISBN-13: 978-3527327614.

A: Gaisford S., Kett V., Haines P.: Principles of Thermal Analysis and Calorimetry, 2nd edition (292 pp). Royal Society for Chemistry (2016), ISBN-13: 978-1-78262-051-8.

Learning resources -
Last update: Leitner Jindřich prof. Ing. DrSc. (25.06.2018)

Powerpoint presentations for lectures.

Technical documentation for used equipment.

Teaching methods -
Last update: Leitner Jindřich prof. Ing. DrSc. (12.09.2018)

Lectures, seminars and individual student work

Syllabus -
Last update: Leitner Jindřich prof. Ing. DrSc. (25.06.2018)

The lecture covers the following topics:

1. Theoretical fundamentals (brief reminders of thermodynamics fundamentals, dependence of thermodynamic functions on temperature, pressure and system composition).

2. Calorimetry and methods of thermal analysis (theoretical basics, instrumentation, interpretation of measured data).

3. Equilibrium measurements (theoretical basics, instrumentation, interpretation of measured data).

4. Other methods (eg determination of surface energy of solids).

Within the experimental part of the workshop students will carry out the measurements with samples of various solids (metals and their alloys, inorganic non-metallic materials and organic polymer materials). The preparation of these samples and their characterization before and after measurements are included.

Course completion requirements -
Last update: Leitner Jindřich prof. Ing. DrSc. (25.06.2018)

Passing the oral examination and processing the protocol for the measurements.

Coursework assessment
Form Significance
Report from individual projects 50
Oral examination 50

 
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