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Students will gain new information on modern separation techniques, specifically liquid, gas, and supercritical chromatography, capillary electrophoresis, and mass spectrometry. Principles of the methods will be summarized. Potential of modern instrumentation for solution of complex analytical tasks will be demonstrated with the emphasis on multidimensional separations. Each student will receive a specific topic to cover in its bibliographic search and he/she will prepare presentation for the peers.
Last update: Sýkora David (03.05.2022)
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Students will gain: new knowledge in the area of up-to-date separation methods insight to the analysis of complex samples utilizing advanced separation methods abilities related with elaboration of a bibliographical search and its prezentation Last update: Sýkora David (03.05.2022)
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The final assessment is based on the evaluation of written test exam and quality of individual bibliography search project including presentation. Last update: Sýkora David (01.09.2018)
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A:Two-Dimensional Liquid Chromatography - firemní příručka. P.W. Carr, D.R. Stoll, Agilent, 2016. A:High Performance Capillary Electrophoresis - D.N. Heiger, Agilent, 2000. A:Introduction to Modern Liquid Chromatography - book, L.R. Snyder, J.J. Kirkland and J.W. Dolan, Wiley, 2010, ISBN:978-0-470-16754-0. A:Gas Chromatography and Mass Spectrometry-A Practical Guide - book, O.D. Sparkman, Z.E. Penton, and F.G. Kitson, 2011, Elsevier, ISBN:978-0-12-373628-4. A:Introduction to Mass Spectrometry - book, J.T. Watson and O.D. Sparkman, Wiley, 2007, ISBN: 978-0-470-51634-8. Last update: Sýkora David (03.05.2022)
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Lectures, seminars, practical demonstrations, presentations. Last update: Sýkora David (31.08.2018)
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1) Principles of gas (GC), liquid (LC) and supercritical fluid chromatography 2) Principles of capillary electrophoresis (CE) a mass spectrometry (MS) 3) Multidimensional techniques of GC I 4) Multidimensional techniques of GC II 5) Multidimensional techniques of GC III 6) Multidimensional techniques of LC I 7) Multidimensional techniques of LC II 8) Multidimensional techniques of LC III 9) Case studies in the forensic analysis 10) Case studies in the analysis of pharmaceuticals 11) Modern chiral separations in the field of CE 12) Chiral selectors in CE 13) Presentation of bibliography search projects I 14) Presentation of bibliography search projects II Last update: Sýkora David (03.05.2022)
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Separation methods - graduate level. Last update: Sýkora David (31.08.2018)
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Analytical chemistry - bachelor's level. Last update: Sýkora David (31.08.2018)
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