SubjectsSubjects(version: 965)
Course, academic year 2019/2020
  
Analytical Chemistry I - S402002
Title: Analytical Chemistry I
Guaranteed by: Department of Analytical Chemistry (402)
Faculty: Faculty of Chemical Engineering
Actual: from 2012 to 2020
Semester: summer
Points: summer s.:5
E-Credits: summer s.:5
Examination process: summer s.:
Hours per week, examination: summer s.:2/2, C+Ex [HT]
Capacity: 10 / 10 (unknown)
Min. number of students: unlimited
State of the course: taught
Language: English
Teaching methods: full-time
Level:  
Guarantor: Setnička Vladimír prof. Ing. Ph.D.
Mestek Oto prof. Ing. CSc.
In complex pre-requisite: N323003
Examination dates   Schedule   
Annotation -
Lectured methods include both classical chemical as well as instrumental techniques. The electrochemical analysis (potentiometry, voltammetry, polarography, coulometry), separation methods (gas and liquid chromatography, electrophoresis) and atomic and molecular spectroscopy (atomic absorption and/or emission spectroscopy, infrared, visible and UV absorption spectroscopy, nuclear magnetic resonance spectrometry) are lectured. Separate lecture is devoted to mass spectrometry and another one to quality assurance procedures in analytical chemistry. The seminars are focused on gravimetric and titration calculations, calculation of equilibria, using of Nernst and/or Lambert-Beers Law and evaluation of basic characteristics of separation processes. The Analytical chemistry I is followed by Analytical chemistry II in next semester, which is application oriented.
Last update: TAJ402 (14.11.2012)
Literature -

Z: D. Kealey, P. J. Haines: Analytical Chemistry, BIOS Sci. Publ., Oxford 2002, ISBN 1-85996-189-4

Last update: TAJ402 (14.11.2012)
Teaching methods -

Every week there is a two hour lecture and two hour seminar. The lectures are concerned about principles, methods and theory. The seminars include practical calculations of titration and gravimetric stoichiometry and pH, complex stability, Nernst and Lambert-Beers Law and evaluation of basic characteristics of separation processes important for analytical chemistry.

Last update: MESTEKO (31.08.2020)
Syllabus -

1. Basic terms in analytical chemistry, equilibria in aqueous solutions

2. Equilibria in aqueous solutions, pH

3. Volumetric and gravimetric analysis

4. Electroanalytical methods

5. Electroanalytical methods

6. Principles of spectrometry, spectrometric instrumentation

7. Atomic spectrometry

8. Molecular spectrometry

9. Molecular spectrometry

10. Extraction, principles of chromatography

11. Principles of chromatography, gas chromatography

12. Liquid chromatography, electrophoresis

13. Mass spectrometry

14. Errors of analytical measurements

Last update: MESTEKO (09.01.2015)
Learning resources -

http://vydavatelstvi.vscht.cz/knihy/uid_es-004

http://vydavatelstvi.vscht.cz/katalog/uid_isbn-978-80-7080-743-9

Last update: TAJ402 (01.10.2013)
Learning outcomes -

The aim of Analytical chemistry I is for studentto learn student analytical chemistry of basic level. Such student shall be able to specify his or her needs when communicating with analytical chemists or shall be able to perform analysis after enhancement of his/her knowledge of specific analytical technique.

Last update: VED402 (16.12.2013)
Entry requirements -

The student needs to know both inorganic and organic chemistry nomenclature, physical principles (magnetism, electromagnetic radiation etc.) and mathematics (polynomials). Sound knowledge in computing with logarithms and percents is essential.

Last update: MESTEKO (08.11.2012)
Registration requirements -

The student needs to know both inorganic and organic chemistry nomenclature, physical principles (magnetism, electromagnetic radiation etc.) and mathematics (polynomials). Sound knowledge in computing with logarithms and percents is essential.

Last update: TAJ402 (01.10.2013)
Teaching methods
Activity Credits Hours
Konzultace s vyučujícími 0.5 14
Účast na přednáškách 1 28
Příprava na přednášky, semináře, laboratoře, exkurzi nebo praxi 1 28
Příprava na zkoušku a její absolvování 1.5 42
Účast na seminářích 1 28
5 / 5 140 / 140
Coursework assessment
Form Significance
Examination test 50
Continuous assessment of study performance and course -credit tests 50

 
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