SubjectsSubjects(version: 855)
Course, academic year 2019/2020
  
Analytical Chemistry II - S402004
Title: Analytical Chemistry II
Guaranteed by: Department of Analytical Chemistry (402)
Actual: from 2019
Semester: winter
Points: winter s.:4
E-Credits: winter s.:4
Examination process: winter s.:
Hours per week, examination: winter s.:2/1 C+Ex [hours/week]
Capacity: unlimited / unlimited (unknown)
Min. number of students: unlimited
Language: English
Teaching methods: full-time
Level:  
For type:  
Additional information: http://www.vscht.cz/anl/pan2/
http://www.vscht.cz/anl/cach2/
Guarantor: Záruba Kamil doc. Ing. Ph.D.
This subject contains the following additional online materials
Annotation
Last update: Záruba Kamil doc. Ing. Ph.D. (02.08.2016)
Lectures of Analytical Chemistry II extend and complement the basic overview of the methods discussed in the course Analytical Chemistry I. They focus primarily on understanding the principles of modern methods of instrumental analysis. The exercises are divided into two sections. The first involves the uncertainty of the quantitative analysis, the other is focused on the foundations of structural analysis - infrared spectrometry, proton NMR spectrometry, and mass spectrometry spectra will be solved.
Aim of the course
Last update: Záruba Kamil doc. Ing. Ph.D. (02.08.2016)

The goal of Analytical chemistry II is to provide

  • orientation in methods of instrumental analysis
  • solve problems of real sample analysis
  • evaluate quality and reliability of analytical results
  • solve simple spectra measured by IR, H-NMR and MS
Literature
Last update: Záruba Kamil doc. Ing. Ph.D. (02.08.2016)

1. PDFs of lectures

2. Skoog, Holler, Nieman, Principles of Instrumental Analysis, Brooks/Cole Thomson Learning

3. Skoog, West, Holler, Crouch, Fundamentals of Analytical Chemistry, Brooks/Cole Thomson Learning

Learning resources
Last update: Řezanka Pavel doc. RNDr. Ing. Ph.D. (07.11.2012)

Recommended during the lectures.

Teaching methods
Last update: Záruba Kamil doc. Ing. Ph.D. (02.08.2016)

Every week of the winter semester there is a two hour lecture and one hour seminar. The lectures are concerned about principles, methods and theory. The seminars include practical calculations and solving of spectra. All seminars are held in computer laboratory.

Requirements to the exam
Last update: Záruba Kamil doc. Ing. Ph.D. (01.07.2019)

1. The credit test is written during seminars in the 7th and 14th week. To get credits, a student has to obtain 50 % of the sum of the tests and 25 % of each test.

2. Students, who study in Czech, pass credit test in Czech. Students, who study in English, pass credit test in English.

3. It is necessary to have the Index (Study Record Book) with yourself during the writing of credit test. Exceptionally, the assistant can allow writing the test after checking the identity of the student using other ID with an up-to-date photograph.

4. Students register for a test using Educational Info System (student.vscht.cz, SIS) and it is the duty of each student to sign in for the term listed there. Signing off is possible up to date listed in SIS. Later, it is possible only by request to the secretary of the department and only because of serious reasons. The test is failed when a student is absent and not signed off.

5. The assistant can allow writing the test when students arrive late. The missed time is not compensated.

6. It is not allowed to leave the room during the test. It is not allowed to use forbidden materials and other tools including telecommunication electronics.

7. Results of the test will be available in place and at the time, which will be announced at the beginning of the test.

8. The credits are written into the Index by the assistant teaching seminars at the appointed time, which will be announced. Exceptionally, it is possible to arrange another time.

9. You can check your test at the assistant teaching seminars in place and at the time, which he or she assigns.

10. The examination is written and takes 50 min. It consists of ten questions. Examiner is allowed to ask further questions.

11. If some of the topics will not be given because of a holiday or a rector’s day, this is not a reason for exclusion of these topics from the examination test.

12. Students, who study in Czech, pass the examination in Czech. Students, who study in English, pass the examination in English.

13. The student has a duty to present the Index with written credits during the examination, otherwise, it is impossible to start/continue the exam.

14. The students sign in for the examination using SIS and it is the duty of a student to sign in for the term listed here. Signing off is possible up to date listed in SIS. Later it is possible only by request to the secretary of the department and only because of serious reasons. The examination is classified „F“ when the student is absent and not signed off.

15. The assistant can allow writing examination when students arrive late. The missed time is not compensated.

16. It is not allowed to leave the room during the examination. It is not allowed to use forbidden materials and tools including telecommunication electronics.

17. The place and time will be announced during the examination. The examiner assigns where and when will be possible to see checked examination test. If the student is not present at this time he or she resigns for any complaint and agree with the final classification. When the student does not agree with the classification of any of parts of the test, the examiner will provide one, exceptionally, more additional questions which will be answered in written form. According to the result of these additional questions, the examiner can change the overall classification.

18. Students can use only two reparative terms.

Syllabus -
Last update: Záruba Kamil doc. Ing. Ph.D. (24.08.2016)

1. Uncertainties and testing of hypotheses in analytical chemistry

2. Vibrational spectrometry - reflection IR, IR microscopy, NIR spectrometry, Raman spectrometry

3. NMR spectrometry - relaxation, chemical exchange, NMR imaging

4. Enhanced mass spectrometry

5. Hyphenated techniques 1 - GC-MS, LC-MS, CE-MS

6. Hyphenated techniques 2 - GC/LC-ICP-MS, speciation analysis; LC/GC-IR, LC-NMR

7. Surface analysis 1 - by photons, electrons, ions

8. Surface analysis 2 - by a probe (STM, AFM, SNOM)

9. Analysis of chiral compounds - Introduction to chiral separation and chiroptic methods

10. Kinetic methods of analysis

11. Radioanalytical methods

12. Biochemical analysis

13. Chemical sensors and biosensors

14. Process analysis

Entry requirements
Last update: Záruba Kamil doc. Ing. Ph.D. (01.07.2019)

The students need to know analytical chemistry at the level of Analytical chemistry I (S402002). Sound knowledge of MS Excel 2007 (or later) is essential for seminars.

Registration requirements
Last update: Záruba Kamil doc. Ing. Ph.D. (01.07.2019)

The students need to know analytical chemistry at the level of Analytical chemistry I (S402002). Sound knowledge of MS Excel 2007 (or later) is essential for seminars.

Teaching methods
Activity Credits Hours
Účast na přednáškách 1 28
Příprava na přednášky, semináře, laboratoře, exkurzi nebo praxi 1,5 42
Příprava na zkoušku a její absolvování 1 28
Účast na seminářích 0,5 14
4 / 4 112 / 112
Coursework assessment
Form Significance
Examination test 50
Continuous assessment of study performance and course -credit tests 50

 
VŠCHT Praha