Subjects

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Development and Optimisation of Procedures in Analytical Laboratory - D323020

Title:	Vývoj a optimalizace postupů v analytické laboratoři
Guaranteed by:	Department of Food Analysis and Nutrition (323)
Faculty:	Faculty of Food and Biochemical Technology
Actual:	from 2013 to 2013
Semester:	both
Points:	0
E-Credits:	0
Examination process:
Hours per week, examination:	0/0, other [HT]
Capacity:	winter:unknown / unknown (unknown) summer:unknown / unknown (unknown)
Min. number of students:	unlimited
State of the course:	taught
Language:	Czech
Teaching methods:	full-time
Teaching methods:	full-time
Level:
Note:	course is intended for doctoral students only you can enroll for the course in winter and in summer semester

Guarantor:	Pulkrabová Jana prof. Ing. Ph.D. Poustka Jan prof. Dr. Ing.

Examination dates Schedule

This subject contains the following additional online materials

E-learning course

Annotation -

The course is divided into two parts: 1. The proposal of the project in the field of laboratory work - the specification and evaluation of parameters of analytical procedures, economical balance; 2. The elaboration of the project focused on the overall balance of the practical realization of specific analytical procedures - students are provided with the corresponding project templates.

Last update: Poustka Jan (03.03.2014)

Aim of the course -

Students will be able to:

1. Systematically process and evaluate the parameters of the analytical procedure

2. Systematically process and evaluate the economic indicators of the analytical procedure

3. Evaluate the feasibility and economy of the analytical procedure with regard to the practical requirements

4. Implement innovations in analytical procedures focused on reliability, speed and economy

Last update: Poustka Jan (03.03.2014)

Course completion requirements -

The submission of the prepared project and its defense.

Last update: Poustka Jan (03.03.2014)

Literature -

The scientific publications and technical specifications including economic indicators - individually according to the topic of a given project

Last update: Poustka Jan (03.03.2014)

Syllabus -

1. General strategies of the development and optimization of analytical procedures

2. Materials necessary for the analytical method optimization

3. Ways of the analytical procedure optimization

4. Optimizations of the izolation phase of analytical procedure - solvent extraction

5. Optimizations of the izolation phase of analytical procedure - solvent free extraction

6. Optimizations of the clean-up phase of analytical procedure

7. Optimizations of the instrumental determination - gas chromatography I

8. Optimizations of the instrumental determination - gas chromatography II

9. Optimizations of the instrumental determination - liquid chromatography I

10. Optimizations of the instrumental determination - liquid chromatography II

11. The cost and operational demands of the analytical procedure

12. The project proposal

13. The interim project control

14. The prezentation of the elaborated project and discussion

Last update: Poustka Jan (03.03.2014)

Learning resources -

Students are provided with the corresponding project templates.

Last update: Poustka Jan (28.02.2014)

Registration requirements -

No requirements.

Last update: Poustka Jan (28.02.2014)

Coursework assessment
Form	Significance
Defense of an individual project	100