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Lectured methods include both classical chemical as well as instrumental techniques. The electrochemical analysis (potentiometry, voltammetry, polarography, coulometry), separation methods (gas and liquid chromatography) and atomic and molecular spectroscopy (atomic absorption and/or emission spectroscopy, infrared, visible and UV absorption, spectroscopy, nuclear magnetic resonance spectroscopy) are lectured. Separate lecture is devoted to mass spectrometry and another one to quality assurance procedures in analytical chemistry. The seminars are focused on gravimetric and titration calculations, calculation of equilibria, using of Nernst and/or Lambert-Beers Law and evaluation of basic characteristics of separation processes. The Analytical chemistry I is followed by Analytical chemistry II in next semester, which is application oriented.
Last update: TAJ402 (23.01.2008)
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The aim of Analytical chemistry I is for student to learn analytical chemistry at basic level. Such student shall be able to specify his or her needs when communicating with analytical chemists or shall be able to perform analysis after enhancement of his/her knowledge of specific analytical technique. Last update: VED402 (16.12.2013)
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Skripta (czech): K. Záruba a kol., Analytická chemie, 1. a 2. díl, Vydavatelstvní VŠCHT Praha, 2016 R: D. Kealey, P. J. Haines: Analytical Chemistry, BIOS Sci. Publ., Oxford 2002, ISBN 1-85996-189-4 Last update: Záruba Kamil (13.01.2017)
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Every week there is a two hour lecture and one hour seminar. The lectures are concerned about principles, methods and theory. The seminars include practical calculations of titration and gravimetric stoichiometry and pH, complex stability and other equlibria important for analytical chemistry. Last update: TAJ402 (23.01.2008)
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1. Basic terms in analytical chemistry, equilibria in aqueous solutions 2. Equilibria in aqueous solutions, pH 3. Volumetric and gravimetric analysis 4. Electroanalytical methods 5. Electroanalytical methods 6. Principles of spectrometry, spectrometric instrumentation 7. Atomic spectrometry 8. Molecular spectrometry 9. Molecular spectrometry 10. Extraction, principles of chromatography 11. Principles of chromatography, gas chromatography 12. Liquid chromatography, electrophoresis 13. Mass spectrometry 14. Errors of analytical measurements
Last update: MESTEKO (09.01.2015)
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http://vydavatelstvi.vscht.cz/knihy/uid_es-004 http://vydavatelstvi.vscht.cz/katalog/uid_isbn-978-80-7080-743-9 Last update: VED402 (02.10.2013)
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The student needs to know both inorganic and organic chemistry nomenclature, physical principles (magnetism, electromagnetic radiation etc.) and mathematics (polynomials). Sound knowledge in computing with logarithms and percents is essential. Last update: TAJ402 (23.01.2008)
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No Last update: VED402 (12.09.2013)
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| Teaching methods | ||||
| Activity | Credits | Hours | ||
| Konzultace s vyučujícími | 0.5 | 14 | ||
| Účast na přednáškách | 1 | 28 | ||
| Příprava na přednášky, semináře, laboratoře, exkurzi nebo praxi | 1 | 28 | ||
| Příprava na zkoušku a její absolvování | 1.5 | 42 | ||
| Účast na seminářích | 1 | 28 | ||
| 5 / 5 | 140 / 140 | |||
| Coursework assessment | |
| Form | Significance |
| Examination test | 50 |
| Continuous assessment of study performance and course -credit tests | 50 |