Subjects

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Analytical Chemistry: Laboratory I - N402003

Title:	Laboratoř analytické chemie I
Guaranteed by:	Department of Analytical Chemistry (402)
Faculty:	Faculty of Chemical Engineering
Actual:	from 2011 to 2018
Semester:	winter
Points:	winter s.:4
E-Credits:	winter s.:4
Examination process:	winter s.:
Hours per week, examination:	winter s.:0/5, MC [HT]
Capacity:	unknown / 180 (unknown)
Min. number of students:	unlimited
State of the course:	taught
Language:	Czech
Teaching methods:	full-time
Teaching methods:	full-time
Level:
Additional information:	http://www.vscht.cz/anl/lach1/
Note:	course can be enrolled in outside the study plan enabled for web enrollment

Guarantor:	Vosmanská Magda Ing. CSc.
Class:	Základní laboratoře
Interchangeability :	N402003A, N402503
Is interchangeable with:	N402003A, N402503

Examination dates Schedule

Annotation -

The laboratory training is focused on acquiring praxis in analytical laboratory. Students learn how to work in a clean, accurate and correct way. The spectrum of methods includes chemical analysis (1-2 works), electrochemical (2-3), spectrophotometric (2) and separation (1) methods. The Laboratory is followed by Laboratory of Analytical Chemistry II.

Last update: Vosmanská Magda (29.05.2019)

Aim of the course -

Students will be able to:

do basic laboratory analytical operations

manipulate with different types of electrodes

work with spectrophotometer and liquid chromatograph

evaluate the results of the measurements

Last update: Vosmanská Magda (29.05.2019)

Literature -

Manuals are availabe for download at https://uanlch.vscht.cz/studium/bakalarske/laboratore/lachi

Last update: Vosmanská Magda (29.05.2019)

Teaching methods -

Laboratory praxis.

Last update: Vosmanská Magda (29.05.2019)

Requirements to the exam -

The every laboratory starts with 5-minute 6-question test, to prove that student read the manual and is able to work safely and purposefully. The 3 questions need to be answered correctly to be allowed to work. If not, the test is classified F. Every work is classified after delivering of report or not classified if report is not delivered or delivered late. If the report was delivered in time and was not classified, the protocol needs to be corrected, in such case contact your teaching assistant. The overall classification is the arithmetic average off all marks, including all F for unsuccessful tests. To obtain final mark, all practices need to be passed with maximum two F.

Last update: Vosmanská Magda (29.05.2019)

Syllabus -

1. Gravimetric and chelatometric determination of nickel

2. Determination of fluorides by ISE

3. Potentiometric measurement of pH

4. Coulometric determination of ascorbic acid

5. Spectrophotometric determination of iron with 1,10-fenanthroline

6. Liquid chromatography

7. IR spectroscopy

Last update: Vosmanská Magda (29.05.2019)

Learning resources -

https://uanlch.vscht.cz/studium/bakalarske/laboratore/lachi

Last update: Vosmanská Magda (29.05.2019)

Entry requirements -

The previous experience from chemical laboratory of any kind is expected. The knowledge of MS Excel is essential for some of labs (charts, basic calculation, working with cell references).

Last update: Vosmanská Magda (29.05.2019)

Registration requirements -

Last update: Vosmanská Magda (29.05.2019)

Teaching methods
	Activity	Credits	Hours
	Účast v laboratořích (na exkurzi nebo praxi)	2.5	70
	Příprava na přednášky, semináře, laboratoře, exkurzi nebo praxi	0.5	14
		3 / 4	84 / 112

Coursework assessment
Form	Significance
Regular attendance	30
Report from individual projects	50
Continuous assessment of study performance and course -credit tests	20