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The course represents the first part of fundamental concepts of analytical chemistry for the study program CHEMISTRY. The principles of analytical methods are introduced considering the applications in different types of analytical laboratories from routine to scientific ones. Firstly, the classical chemical methods are explained. Secondly, the general concepts of instrumental methods are described with special focus on electrochemistry (potentiometry, voltammetry, polarography, coulometry), separation science (gas and liquid chromatography) and spectroscopy. The course is taught only together with the subsequent course Analytical chemistry B.
Last update: VED402 (16.12.2013)
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Students will be able to: Use fundamental analytical concepts, to describe principles of both qualitative and quantitative chemical analyses, including examples of gravimetric and titrimetric determinations. Describe principles of electroanalytical techniques, to know examples of potentiometric, voltammetric and conductometric determinations. Apply basic principles of separation science focusing on chromatographic and electromigration techniques. Know fundamental concepts of spectroscopic techniques. Last update: VED402 (16.12.2013)
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R:Volka et al. Analytická chemie I, VŠCHT Praha, Praha 1995 (dotisk 1997) R:Volka et al. Analytická chemie II, VŠCHT Praha, Praha 1997 R:D. Kealey, P. J. Haines: Analytical Chemistry, BIOS Sci. Publ., Oxford 2002 A:James W. Robinson, Eileen Mary Skelly Frame, George M. Frame: Undergraduate Instrumental Analysis, Sixth Edition, Marcel Dekker, New York 2005 ISBN: 0-8247-5359-3 A:Francis Rouessac, Annick Rouessa: Chemical Analysis: Modern Instrumentation Methods and Techniques, 2nd Edition, Wiley, Chichester 2007 ISBN: 978-0-470-85903-2 Last update: Matějka Pavel (04.09.2013)
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1. Basic concepts in analytical chemistry 2. Equilibria in aqueous solutions - acid-base, complexometric 3. Equilibria in aqueous solutions - precipitation, redox 4. Chemical qualitative analysis 5. Gravimetric analysis, titrimetric analysis - general principals 6. Titrimetric analysis - acid-base and complexometric titrations 7. Titrimetric analysis - precipitation and redox titrations 8. Introduction to electrochemical methods - basic concepts 9. Potentiometry, voltammetry 10. Introduction to separation methods 11. Gas and liquid chromatography 12. Electromigration methods 13. Introduction to spectrochemical methods 14. Application of Lambert-Beer law Last update: Matějka Pavel (28.08.2013)
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electronic materials for lectures and an overview of seminars http://www.vscht.cz/anl/ach_A_B/ Last update: Matějka Pavel (31.08.2013)
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Introduction to chemistry Physics A Last update: Matějka Pavel (31.08.2013)
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| Teaching methods | ||||
| Activity | Credits | Hours | ||
| Konzultace s vyučujícími | 0.5 | 14 | ||
| Účast na přednáškách | 1 | 28 | ||
| Příprava na přednášky, semináře, laboratoře, exkurzi nebo praxi | 1 | 28 | ||
| Účast na seminářích | 0.5 | 14 | ||
| 3 / 3 | 84 / 84 | |||
| Coursework assessment | |
| Form | Significance |
| Regular attendance | 10 |
| Continuous assessment of study performance and course -credit tests | 90 |