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Theory and Experiment of Separation Methods - N402084

Title:	Teorie a experiment separačních metod
Guaranteed by:	Department of Analytical Chemistry (402)
Faculty:	Faculty of Chemical Engineering
Actual:	from 2013 to 2013
Semester:	winter
Points:	winter s.:4
E-Credits:	winter s.:4
Examination process:	winter s.:
Hours per week, examination:	winter s.:2/1, Ex [HT]
Capacity:	unknown / unknown (unknown)
Min. number of students:	unlimited
State of the course:	taught
Language:	Czech
Teaching methods:	full-time
Teaching methods:	full-time
Level:
Note:	course can be enrolled in outside the study plan enabled for web enrollment

Guarantor:	Sýkora David prof. Dr. RNDr.

Examination dates Schedule

Annotation -

The lectures are focused on separation techniques. Both historically older techniques such as destilation and extraction and modern methods, for example high performance liquid chromatography, capillary electrophoresis, mass spectrometry are presented. Besides well known techniques less common methods that have great separation potencial are also discussed.

Last update: Sýkora David (18.09.2013)

Aim of the course -

Students will know:

basic principles of the frequently used separation techniques.

Last update: Sýkora David (18.09.2013)

Literature -

R: Separace látek - skripta, M. Popl, J. Kubát; SNTL, 1986.

R: High Performance Capillary Electrophoresis - firemní příručka, D.N. Heiger, Hewlett-Packard, 1992.

A: Chromatography Today - kniha, C.F. Poole, S.K. Poole; Elsevier, 1991, ISBN:0-444-88492-0.

A: Chromatographic methods - kniha, A. Braithwaite, F.J. Smith; Blackie Academic & Proffessional, 1996, ISBN:0-7514-0158-7.

A: Gas Chromatography - kniha, I.A. Fowlis; ACOL, Wiley, 1995, ISBN:0-471-95467-5.

A: High Performance Liquid Chromatography - kniha, S. Lindsay; ACOL, Wiley, 1992, ISBN:0-471-93180-2.

A: Practical HPLC Method Development - L.R. Snyder, J.J. Kirkland, J.L. Glajch; Wiley, 1997, ISBN:0-471-00703-X.

Last update: VED402 (01.10.2013)

Teaching methods -

Presentations are continuously modified, various web pages are also used for the education.

Last update: Sýkora David (18.09.2013)

Requirements to the exam - Czech

Přemět je zakončen ústní zkouškou.

Last update: Sýkora David (18.09.2013)

Syllabus -

1. Introduction to Separation Methods

2. Destilations

3. Extractions

4. Separations Based on Phase Equilibria

5. Membrane Separation

6. Separation in Force Field

7. Electrophoresis

8. Capillary Electrophoresis

9. Capillary Electrochromatography

10. Chromatography

11. Gas Chromatography

12. Liquid Chromatography

13. Supercritical Fluid Chromatography

14. Mass spectrometry

Last update: Sýkora David (18.09.2013)

Learning resources -

Electronic version of presentations available for the students.

Last update: Sýkora David (18.09.2013)

Entry requirements -

Basic knowledge of analytical chemistry

Last update: Sýkora David (18.09.2013)

Registration requirements -

None.

Last update: Sýkora David (18.09.2013)

Teaching methods
	Activity	Credits	Hours
	Obhajoba individuálního projektu	0.5	14
	Příprava na zkoušku a její absolvování	3.5	98
		4 / 4	112 / 112

Coursework assessment
Form	Significance
Defense of an individual project	10
Oral examination	90