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The crux of this subject consists in understanding the relation between the physical basis of individual spectroscopic method or technique and their application for study of the physical-chemical properties of substances. The accent will be put on the fact that the results of individual methods are complementary and confirm each other. Interpretation of spectra will be beside the identification of compounds aimed at the study of intermolecular interactions and supramolecular structures. The description of the instrumentation will be limited to basic facts on which the applications are based.
Last update: TAJ403 (13.12.2013)
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Students will able to: Understand the physical principles of spectroscopic methods Apply these physical principles to the selection of methods which are appropriate for the study of the given properties of specific types of compounds Interpret the results of measurements for individual methods Combine the results of individual methods Be familiar with basic instrumentation of methods with respect to resulting applications Last update: TAJ403 (13.12.2013)
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R: Atkins P.W., de Paula J., Physical Chemistry, Oxford University Press, 2010, 9780199543373 A: Gauglitz G., Handbook of Spectroscopy,John Wiley & Sons, 2006, 3527297820 Last update: TAJ403 (10.09.2013)
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1. Introduction, basic concepts, basic principles 2. X-ray fluorescence analysis, photoelectron spectroscopy, Auger spectrosopy 3. Atomic absorption spectrometry, Atomic emission spectrometry 4. UV-VIS spectrosopy, FIA, nephelometry, turbidimetry 5. Luminiscence methods 6. Infrared spectrometry - basic principle, instrumentation and examples of applications 7. Interpretation of IR spectra 8. Raman spectrometry, rotational spectrometry 9. NMR- basic principle, instrumentation and examples of applications 10. Interpretation of NMR spectra 11. ss NMR, basic principle, instrumentation and examples of applications 12. Mass spectrometry, combined techniques 13. Interpretation of mass spectra 14. Chiroptical methods - optical activity, ECD, VCD and ROA, possibilities of NMR for study of optically active compounds Last update: TAJ403 (10.09.2013)
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http://e-knihovna.vscht.cz/admin/default.aspx?page=1&ii=&td=&rok=&lokace=&v=1&p=9&kat=28&stav=*&new=*&od=&do=&rev=&starting=&autor=&nazev=Handbook+of+Spectroscopy
Last update: TAJ403 (10.09.2013)
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Physical chemistry I Last update: TAJ403 (10.09.2013)
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| Teaching methods | ||||
| Activity | Credits | Hours | ||
| Účast na přednáškách | 0.5 | 14 | ||
| Příprava na přednášky, semináře, laboratoře, exkurzi nebo praxi | 1 | 28 | ||
| Příprava na zkoušku a její absolvování | 1 | 28 | ||
| Účast na seminářích | 0.5 | 14 | ||
| 3 / 3 | 84 / 84 | |||
| Coursework assessment | |
| Form | Significance |
| Regular attendance | 20 |
| Examination test | 40 |
| Oral examination | 40 |