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Students will learn the principles of portable analytical methods and their use for analyzes in the field. They learn to choose a suitable analytical method for specific types of samples, learn the principles of correct sampling and in-situ analysis. Students will also acquire practical skills with field analyzers and will be familiar with the basics of safety at work with portable analytic devices.
Last update: Martinec Marek (25.01.2018)
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In order to successfully complete this course, students have to obtain a credit and pass the final exam. To obtain credit, students have to actively participate on all exercises. The credit is obligatory condition for admission to the final exam. The final exam will consist of two parts - a written test and an oral exam. Last update: Martinec Marek (29.01.2018)
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R:KEALEY, D. a P. J. HAINES. Analytical chemistry. Oxford: BIOS, 2002. Instant notes series. ISBN 1-85996-189-4. R:ROBINSON, James W., Eileen M. Skelly FRAME a George M. FRAME. Undergraduate instrumental analysis. 6th ed. /. New York: M. Dekker, c2005. ISBN 0-8247-5359-3. R:ROUESSAC, Francis. a Annick. ROUESSAC. Chemical analysis: modern instrumentation methods and techniques. 2nd ed. Chichester: John Wiley, 2007. ISBN 978-0-470-85903-2. Last update: Martinec Marek (25.01.2018)
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1. Use of portable analyzers in the field 2. Mobile analysis of hazardous gaseous and volatile substances (PID, FID, ...), CHMI (AIM, MIM, ISKO) 3. Multiparametric probes (pH, ORP, conductivity, DO, ISE, optical and electrochemical electrodes) 4. UV-VIS spectrophotometers, field analysis of the composition of liquids 5. Raman spectrometry and portable Raman spectrometers 6. Infrared spectrometry and portable FT-IR and NIR spectrometers 7. Radioactivity and Geiger-Müller counters 8. Portable gamma spectrometers and portable XRF spectrometers 9. Portable GC-MS detectors, gas chromatography and detectors 10. Sampling and adjustment of samples for field measurements and sample transport 11. Field analysis of gases, liquids and solids 12. Field analysis of unknown and dangerous substances, analysis of valuable items and artwork 13. Safety at work with portable analytical devices 14. First aid in the field Last update: Martinec Marek (29.01.2018)
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https://uchop.vscht.cz/predmety/portables Last update: Martinec Marek (25.01.2018)
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Students will be able to: Orient in portable instrumental analytical methods. Know basic principles of spectral methods and interpretation of acquired spectra. Evaluate the quality and reliability of analytical results. Know the principles of sampling for field analysis and transport to the laboratory. Solve specific problems of real sample analysis. Know the basic principles of work safety with portable analytical instruments and the basics of first aid. Last update: Martinec Marek (25.01.2018)
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Passing Analytical Chemistry I and II or Analytical Chemistry A and B Last update: Martinec Marek (25.01.2018)
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General and inorganic chemistry Organic chemistry Physics Physical chemistry Last update: Martinec Marek (25.01.2018)
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Teaching methods | ||||
Activity | Credits | Hours | ||
Účast na přednáškách | 0.5 | 14 | ||
Příprava na zkoušku a její absolvování | 2 | 56 | ||
Účast na seminářích | 1.5 | 42 | ||
4 / 4 | 112 / 112 |
Coursework assessment | |
Form | Significance |
Examination test | 50 |
Continuous assessment of study performance and course -credit tests | 25 |
Oral examination | 25 |