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Course is focused on basic methods of analysis of elements: chemical analysis (titration, gravimetric, photometric method), spectrometric methods (atomic absorption, fluorescence, emission and mass spectrometry) and electrochemical methods (potentiometry, voltammetry). Attention is also paid to the preparation of samples for analysis.
Last update: MESTEKO (23.01.2018)
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Pro splnění ústní zkoušky musí student úspěšně zodpovědět dvě otázky ze seznamu otázek. Last update: MESTEKO (22.02.2018)
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R: Cullen M.: Atomic Spectroscopy in Elemental Analysis, Blackwell, ISBN 1-84127-333-3 R: Skoog D.A., West D.M., Holler F.J.: Fundamentals of Analytical Chemistry, 7. nebo novější vydání, Saunders College Publishing, ISBN 0-03-38-005938-0 Skripta (czech): K. Záruba a kol., Analytická chemie, 1. díl, Vydavatelstvní VŠCHT Praha, 2016, ISBN 978-80-7080-950-1 K. Záruba a kol., Analytická chemie, 2. díl, Vydavatelstvní VŠCHT Praha, 2016, ISBN 978-80-7080-951-1 Skripta (in Czech): Černohorský T., Jandera P.: Atomová spektroskopie, Univerzita Pardubice 1997. ISBN 80-7194-114-X R: Ebdon L., Evans E.H., Fisher A.S., Hill S.J.: An Introduction to Analytical Atomic Spectrometry. Willey 1998, ISBN 978-0-471-97418-5 Last update: MESTEKO (20.02.2018)
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Students complete oral exam. Last update: MESTEKO (23.01.2018)
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1 Gravimetry 2 Titrimetry: acidimetry anad alkalimetry, chelatometry, argentometry 3 Titrimetry: oxidimetry 4 Photometry 5 Atomic absorption spektrometry with flame atomisation 6 Atomic absorption spektrometry with electrotermic atomisation 7 Atomic fluorescence spektrometry and flame emission spectrometry 8 Inductively coupled plasma optical emission spectrometry 9 Inductively coupled plasma mass spectrometry 10 Speciation analysis of trace elements 11 Potentiometry, pH determination, ion selective electrodes 12 Coulometry 13 Voltametry, polarography 14 Sample preparation and experiments in elemental analysis Last update: MESTEKO (23.01.2018)
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http://web.vscht.cz/~koplikr/Atomov%c3%a1%20%20spektrometrie.pdf Last update: Pátková Vlasta (05.01.2018)
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Students gain theoretical knowledge of various methods of elemental analysis: gravimetric and titration methods, optical spectroscopy (absorption, fluorescence and emission spectrometry), mass spectrometry and electroanalytical methods. Become familiar with the techniques of preparation of samples for analysis and the issue of ensuring clean environment in the trace lab. In addition to determining the total element concentrations, they are also familiar with the methods of speciation analysis using a combination of spectral and separation methods. Last update: MESTEKO (23.01.2018)
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Basic knowledge of analytical chemistry Last update: Pátková Vlasta (05.01.2018)
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Teaching methods | ||||
Activity | Credits | Hours | ||
Konzultace s vyučujícími | 0.2 | 6 | ||
Účast na přednáškách | 1 | 28 | ||
Příprava na přednášky, semináře, laboratoře, exkurzi nebo praxi | 0.5 | 14 | ||
Příprava na zkoušku a její absolvování | 1.3 | 36 | ||
3 / 3 | 84 / 84 |
Coursework assessment | |
Form | Significance |
Oral examination | 100 |