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Students will learn about laboratory safety, basic laboratory equipment and experimental procedures used in inorganic and organic chemistry. Preparations and qualitative reactions will complement the theoretical knowledge of properties of elements and inorganic compounds. Working on several simple organic syntheses, students will acquire the requisite skills for the preparation and characterization of organic compounds. Final grade is based not only on the performance in the laboratory, but also on the knowledge of simple calculations (stoichiometry and preparation of solutions) and the chemical principles of procedures carried out.
Last update: MARTINUT (02.08.2013)
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R: Dagmar Sýkorová, Libor Mastný: Návody pro laboratoře z anorganické chemie, VŠCHT Praha, 2001, dotisk 2009, 9788070804520 R: V.Flemr, E. Holečková: Úlohy z názvosloví a chemických výpočtů v anorganické chemii,VŠCHT Praha, 2001, 8070804351 A: F.Jursík, Anorganická chemie nekovů, VŠCHT Praha, 2001, 8070804173 A: F.Jursík,Anorganická chemie kovů, VŠCHT Praha, 2003, 8070805048 R: Šilhánková a kol.: Laboratoř organické chemie, VŠCHT Praha, 2000, dotisk 2007, 8070803959 Last update: Cibulka Radek (28.08.2013)
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1. Laboratory safety, rules, and protocols. 2. Basic inorganic laboratory equipment. 3. Basic laboratory procedures - dissolution, filtration, evaporation, precipitation, and decantation. 4. Basic laboratory operations - crystallization, weighing, determination of density, pH measurement. 5. Redox reactions - carrying out in solution and solid phase. 6. Chemistry of nonmetals - reactions of nonmetals and their compounds. 7. Important qualitative reactions of selected anions, their determination in an unknown sample. 8. Basic organic laboratory equipment. 9. Building of reaction apparatuses and basic operations in organic synthesis. 10. Selected one-step organic syntheses including isolation and identification of products, heating with stirring under a reflux condenser. 11. Crystallization in organic laboratory. 12. Extraction. 13. Distillation under ambient pressure. 14. Determination of melting point, GLC chromatography of compounds prepared. Last update: MARTINUT (02.08.2013)
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Laboratory instructions Last update: MARTINUT (02.08.2013)
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Students will be able to: work safely in a laboratory carry out basic laboratory operations combine the theoretical knowledge with experimental results understand the principles of organic synthesis - planning, building a reaction apparatus, carrying out a reaction, isolation and characterization of products write laboratory protocols Last update: Cibulka Radek (22.08.2013)
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Organic Chemistry I Last update: Cibulka Radek (28.08.2013)
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