Subjects

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Analytical Chemistry A - N402051

Title:	Analytická chemie A
Guaranteed by:	Department of Analytical Chemistry (402)
Faculty:	Faculty of Chemical Engineering
Actual:	from 2019 to 2019
Semester:	winter
Points:	winter s.:3
E-Credits:	winter s.:3
Examination process:	winter s.:
Hours per week, examination:	winter s.:2/1, MC [HT]
Capacity:	unknown / unlimited (unknown)
Min. number of students:	unlimited
State of the course:	taught
Language:	Czech
Teaching methods:	full-time
Level:
Additional information:	https://e-learning.vscht.cz/

Guarantor:	Matějka Pavel prof. Dr. RNDr.
In complex pre-requisite:	N323003

Examination dates Schedule

Annotation -

The course represents the first part of fundamental concepts of analytical chemistry for the study program CHEMISTRY. The principles of analytical methods are introduced considering the applications in different types of analytical laboratories from routine to scientific ones. Firstly, the classical chemical methods are explained. Secondly, the general concepts of instrumental methods are described with special focus on electrochemistry (potentiometry, voltammetry, polarography, coulometry), separation science (gas and liquid chromatography) and spectroscopy. The course is taught only together with the subsequent course Analytical chemistry B.

Last update: VED402 (16.12.2013)

Literature -

R:Volka et al. Analytická chemie I, VŠCHT Praha, Praha 1995 (dotisk 1997)

R:Volka et al. Analytická chemie II, VŠCHT Praha, Praha 1997

R:D. Kealey, P. J. Haines: Analytical Chemistry, BIOS Sci. Publ., Oxford 2002

A:James W. Robinson, Eileen Mary Skelly Frame, George M. Frame: Undergraduate Instrumental Analysis, Sixth Edition, Marcel Dekker, New York 2005 ISBN: 0-8247-5359-3

A:Francis Rouessac, Annick Rouessa: Chemical Analysis: Modern Instrumentation Methods and Techniques, 2nd Edition, Wiley, Chichester 2007 ISBN: 978-0-470-85903-2

Last update: Matějka Pavel (04.09.2013)

Syllabus -

1. Basic concepts in analytical chemistry

2. Equilibria in aqueous solutions - acid-base, complexometric

3. Equilibria in aqueous solutions - precipitation, redox

4. Chemical qualitative analysis

5. Gravimetric analysis, titrimetric analysis - general principals

6. Titrimetric analysis - acid-base and complexometric titrations

7. Titrimetric analysis - precipitation and redox titrations

8. Introduction to electrochemical methods - basic concepts

9. Potentiometry, voltammetry

10. Introduction to separation methods

11. Gas and liquid chromatography

12. Electromigration methods

13. Introduction to spectrochemical methods

14. Application of Lambert-Beer law

Last update: Matějka Pavel (28.08.2013)

Learning resources -

electronic materials for lectures and an overview of seminars http://www.vscht.cz/anl/ach_A_B/

Last update: Matějka Pavel (31.08.2013)

Learning outcomes -

Students will be able to:

Use fundamental analytical concepts, to describe principles of both qualitative and quantitative chemical analyses, including examples of gravimetric and titrimetric determinations.

Describe principles of electroanalytical techniques, to know examples of potentiometric, voltammetric and conductometric determinations.

Apply basic principles of separation science focusing on chromatographic and electromigration techniques.

Know fundamental concepts of spectroscopic techniques.

Last update: VED402 (16.12.2013)

Registration requirements -

Introduction to chemistry

Physics A

Last update: Matějka Pavel (31.08.2013)

Teaching methods
	Activity	Credits	Hours
	Konzultace s vyučujícími	0.5	14
	Účast na přednáškách	1	28
	Příprava na přednášky, semináře, laboratoře, exkurzi nebo praxi	1	28
	Účast na seminářích	0.5	14
		3 / 3	84 / 84

Coursework assessment
Form	Significance
Regular attendance	10
Continuous assessment of study performance and course -credit tests	90