Subjects

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Structural Analysis - AM110020

Title:	Structural Analysis
Guaranteed by:	Department of Organic Chemistry (110)
Faculty:	Faculty of Chemical Technology
Actual:	from 2020 to 2020
Semester:	summer
Points:	summer s.:4
E-Credits:	summer s.:4
Examination process:	summer s.:
Hours per week, examination:	summer s.:2/1, C+Ex [HT]
Capacity:	unlimited / unlimited (unknown)
Min. number of students:	unlimited
State of the course:	taught
Language:	English
Teaching methods:	full-time
Teaching methods:	full-time
Level:
Note:	course can be enrolled in outside the study plan enabled for web enrollment

Guarantor:	Kohout Michal prof. Ing. Ph.D.
Classification:	Chemistry > Analytical Chemistry

Examination dates Schedule

Annotation -

The aim of the subject is to introduce to students the principles of basic spectral methods and their application in organic chemistry.

Last update: Kohout Michal (02.11.2019)

Aim of the course -

Students will be able to :

determine a structure of a molecule from spectra thanks to thorough training in:

1H and 13C NMR spectroscopy and basic 2D methods (COSY, HSQC, HMBC)

infrared spectroscopy

UV/Vis spectroscopy

mass spectrometry

Last update: Kohout Michal (02.11.2019)

Literature -

Williams D.H., Fleming I.: Spectroscopic methods in organic chemistry. 5. vydání. DH Williams & I Fleming.

Richards S.A., Hollerton J.C.: Essential Practical NMR for Organic Chemistry. 2011 John Wiley & Sons, Ltd.

Last update: Kohout Michal (20.10.2019)

Syllabus -

1. The introduction to molecular spectroscopy, basic terms and principles.

2. NMR spectroscopy, background, basic terms and the utilization area.

3. 1H NMR in organic structural analysis.

4. 13C NMR in organic structural analysis.

5. Special NMR techniques.

6. Two-dimensional NMR spectroscopy, COSY, HETCOR.

7. Infrared spectroscopy, basic terms and principles of the method.

8. Area of characteristic vibrations and the fingerprint region.

9. Possibilities of practical applications in structural analysis.

10. UV-VIS spectroscopy, basic terms and principles of the method.

11. Practical application of UV-VIS in structural analysis.

12. Mass spectrometry, principles of the method, experimental set-up.

13. Ionization techniques, sample preparation, basic principles of fragmentation.

14. Practical application of MS in structural analysis of organic molecules.

Last update: Kohout Michal (02.11.2019)

Learning resources -

Materials from the lecturer available on-line via an e-learning portal.

Last update: Kohout Michal (02.11.2019)

Registration requirements -

Organic Chemistry II, Physics

Last update: Kohout Michal (02.11.2019)